Doping and Photocatalytic Performance of TiO2 Nanopowder: An Inorganic Comprehensive Experiment for Boling Class

B. Zhu, 天津 sup 南开大学化学学院, Shasha Zhang, Guona Huo, Lulu Ma, Zhenning Li, Zhenxiang Zhao, Qijie Shen, Xiaohang Qiu, 天津 sup 化学国家级实验教学示范中心
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Abstract

An experiment “Doping and Photocatalytic Performance of TiO2 Nanopowder” was performed in inorganic comprehensive laboratory for Boling Class of Nankai University. After the dopant precursors and corresponding contents were determined by the students, different elements doped TiO2 powders were prepared by sol-gel method, and characterized by scanning electronic microscopy, transmittance electronic microscopy, powder X-ray diffraction and UV-Vis diffuse reflectance spectroscopy. The photocatalytic performances of the prepared catalysts were monitored by the degradation of methyl orange as the simulated wastewater to select the superior ones for photocatalytic water splitting test. Through this comprehensive experiment related to research frontier, the students in Boling Class can obtain basic research training and their scientific literacy can be improved.
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二氧化钛纳米粉体的掺杂与光催化性能:玻林类无机综合实验
在南开大学博灵班无机综合实验室进行了“TiO2纳米粉体的掺杂与光催化性能”实验。在学生确定了掺杂前驱物及其含量后,采用溶胶-凝胶法制备了不同元素掺杂的TiO2粉末,并通过扫描电镜、透射电镜、粉末x射线衍射和UV-Vis漫反射光谱对其进行了表征。以甲基橙降解为模拟废水,对制备的催化剂进行光催化性能监测,筛选出性能较好的催化剂进行光催化水分解试验。通过这一与研究前沿相关的综合性实验,使班学生获得基础研究训练,提高科学素养。
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