Soft mechanochemical synthesis and characterization of nanodimensional spinel ferrites

Z. Lazarević, A. Milutinović, M. Romčević, N. Romčević, Č. Jovalekić, D. Sekulić, M. Slankamenac
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引用次数: 1

Abstract

NiFe2O4 and ZnFe2O4 ferrites have been prepared by soft mechanochemical synthesis. The sintered samples were analyzed by XRD and Raman spectroscopy. Investigation of the magnetization as a function of magnetic field confirms an expected change of the degree of inversion in the spinel structure with the sintering. Impedance spectroscopy on the sintered pellets of ferrites was performed in the wide frequency range (100 Hz-10 MHz) at different temperatures using an Impedance/Gain-Phase Analyzer (HP-4194).
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纳米尖晶石铁氧体的软机械化学合成与表征
采用软机械化学合成方法制备了NiFe2O4和ZnFe2O4铁氧体。采用XRD和拉曼光谱对烧结样品进行了分析。磁化强度随磁场变化的研究证实了尖晶石结构反转程度随烧结的变化。利用阻抗/增益相位分析仪(HP-4194)对烧结铁氧体球团在不同温度下的宽频率范围(100 Hz-10 MHz)进行阻抗谱分析。
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