Separation Process of Citronellal and Rhodinol from Citronella Oil using Vacuum Fractionations at Pilot Plant Scale

Risna Silvianti, .. Warsito, C. Cahyani
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Abstract

: The aim of this work was to separate major components from citronella oil using vacuum distillation fractionation method. Operating condition that used in this study is vacuum pressure 10-30 mmHg. This process depends on the pressure and temperature of the system, as well the physical and chemical characteristics of the components to be separated.Based on GC-MS analysis of Citronella Oil is known that citronellal, citronellol, and geraniol has yielded 7,42%; 11,25%; and 31,68%, respectively. Fractional distillation under reduced pressure can isolate major component like limonene,citronellal,citronellol and rhodinol with higher purity 55.56%; 25.57%; and 46.19%, respectively .
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真空分馏从香茅油中分离香茅醛和Rhodinol的工艺研究
采用真空蒸馏分馏法对香茅油中的主要成分进行分离。本研究使用的操作条件为真空压力10-30 mmHg。这一过程取决于系统的压力和温度,以及待分离组分的物理和化学特性。通过GC-MS分析可知香茅油中香茅醛、香茅醇、香叶醇的收率为7.42%;11日,25%;31,分别是68%。减压分馏可分离出柠檬烯、香茅醛、香茅醇和rhodinol等主要成分,纯度较高,为55.56%;25.57%;分别为46.19%。
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