Optical and Structural Study of Biocompatible Silver-Chitosan Colloids

Vismitha S. Patil, B. Saraswathi, R. M. Hodlur, J. AmithYadavH., S. V. Halse, Muttanagoud N. Kalasad
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Abstract

Nontoxic and biocompatible silver-chitosan colloids were prepared by direct chemical reduction. The Ag-chitosan colloids are drop cast on a glass slide and left to dry to obtain uniform, homogeneous films. The presence of chitosan prevented the growth of silver nanoparticles from agglomeration. The occurrence of localized surface plasmon resonance (LSPR) at ~ 400 nm in the optical absorption spectra indicated the formation of Ag nanoparticles which is the characteristic property of metal nanoparticles. The -prepared colloidal Ag nanoparticles are chemically stable and remain colloidal even after aging. The estimated average particle size is about 14nm and the face-centered cubic phase was observed in the XRD pattern. SEM images clearly showed the homogeneous distribution of silver nanoparticles.
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生物相容性银壳聚糖胶体的光学和结构研究
采用直接化学还原法制备了无毒、生物相容性好的银壳聚糖胶体。ag -壳聚糖胶体滴投在玻片上,晾干后得到均匀、均匀的薄膜。壳聚糖的存在阻止了银纳米颗粒的团聚生长。光学吸收光谱中~ 400 nm处出现局域表面等离子体共振(LSPR),表明银纳米粒子的形成是金属纳米粒子的特征性质。制备的胶体银纳米颗粒化学性质稳定,即使老化后仍保持胶体状态。平均粒径约为14nm,在XRD图中观察到面心立方相。SEM图像清晰地显示了银纳米颗粒的均匀分布。
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