Structural and Optical Properties of Calcium Titanate Prepared from Gypsum

IF 3.9 Q2 NANOSCIENCE & NANOTECHNOLOGY Journal of Nanotechnology Pub Date : 2022-03-24 DOI:10.1155/2022/6020378
M. Mostafa, Z. Alrowaili, M.M. Al Shehri, M. Mobarak, A. Abbas
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引用次数: 2

Abstract

Ceramic materials have been used in various human health-related applications for considerable time. One of the important applications of ceramic materials is in electronics. Our work focuses on calcium titanate (CaTiO3). CaTiO3 is typically created via sintering. Gypsum particles is used to form calcium hydroxide, which is then combined with titanium dioxide to form rutile crystals. Thereafter, calcination is performed at 900°C, 1000°C, and 1100°C for 2 h. X-ray diffraction is employed to track the evolution of the CaTiO3 phase. Scanning electron microscopy is used to characterize the morphologies of the different preparation steps. As the calcination temperature increases from 900°C to 1000°C, the crystallite size of CaTiO3 increases from 35 nm to 45 nm. Furthermore, the energy gaps of the CaTiO3 powders obtained after calcination at 900°C and 1000°C are 5.32 eV and 5.43 eV, respectively, and their particle sizes are 150–200 nm and 200–300 nm, respectively.
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石膏制备钛酸钙的结构和光学性质
陶瓷材料已用于各种人类健康相关的应用相当长的时间。陶瓷材料的重要应用之一是在电子领域。我们的工作重点是钛酸钙(CaTiO3)。CaTiO3通常是通过烧结产生的。石膏颗粒被用来形成氢氧化钙,然后与二氧化钛结合形成金红石晶体。之后,在900°C、1000°C和1100°C下进行2小时的煅烧。采用x射线衍射法对CaTiO3相的演化过程进行了跟踪。扫描电子显微镜用于表征不同制备步骤的形貌。随着煅烧温度从900℃增加到1000℃,CaTiO3的晶粒尺寸从35 nm增加到45 nm。900℃和1000℃煅烧得到的CaTiO3粉体的能隙分别为5.32 eV和5.43 eV,粒径分别为150 ~ 200 nm和200 ~ 300 nm。
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来源期刊
Journal of Nanotechnology
Journal of Nanotechnology NANOSCIENCE & NANOTECHNOLOGY-
CiteScore
5.50
自引率
2.40%
发文量
25
审稿时长
13 weeks
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