Susceptibility of Ajwa dates (Phoenix dactylifera) to aflatoxin contamination based on liquid chromatography combined with electrospray ionisation-triple quadrupole tandem-mass spectrometry (LC-ESI-MS/MS)

IF 0.7 4区 农林科学 Q4 FOOD SCIENCE & TECHNOLOGY international food research journal Pub Date : 2023-04-28 DOI:10.47836/ifrj.30.2.04
M. Almaghrabi, Michael Morgan
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Abstract

Dates are a staple food across the world because of their religious, cultural, and nutritional importance. There are many different varieties of dates, one of which is the Ajwa variety. There have been no reports on the contamination of Ajwa dates by aflatoxins (AFs). Therefore, the present work was conducted to investigate the incidence of AFs in Ajwa dates for the first time. Samples (100) were analysed for AFs using liquid chromatography combined with electrospray ionisation-triple quadrupole tandem-mass spectrometry (LC-ESI-MS/MS). The method was validated and regarded as reliable due to good linearity (R2 > 0.99), satisfactory recovery (61.4 - 105.7%), precision (RSDs ≤ 12.29%), and sensitivity (LOD in the range of 0.042 - 0.013 μg/kg; LOQ in the range of 0.125 - 0.038 μg/kg). Surprisingly, no aflatoxins were detected, which might indicate that this popular type of date is not likely to pose potential health risks, though further research is required.
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基于液相色谱-电喷雾电离-三重四极杆串联质谱联用(LC-ESI-MS/MS)的Ajwa枣对黄曲霉毒素污染敏感性研究
由于其宗教、文化和营养的重要性,枣在世界各地都是一种主食。有许多不同品种的枣,其中之一是Ajwa品种。目前还没有黄曲霉毒素(AFs)污染Ajwa枣的报道。因此,本文首次对Ajwa地区的AFs发病率进行了调查。采用液相色谱联用电喷雾电离-三重四极杆串联质谱(LC-ESI-MS/MS)对100份样品进行AFs分析。方法线性良好(R2 > 0.99),回收率(61.4 ~ 105.7%),精密度(rsd≤12.29%),灵敏度(LOD范围为0.042 ~ 0.013 μg/kg;定量限为0.125 ~ 0.038 μg/kg)。令人惊讶的是,没有检测到黄曲霉毒素,这可能表明这种受欢迎的枣不太可能造成潜在的健康风险,尽管还需要进一步的研究。
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来源期刊
international food research journal
international food research journal Agricultural and Biological Sciences-Food Science
CiteScore
1.40
自引率
0.00%
发文量
75
期刊介绍: The International Food Research Journal (IFRJ) publishes papers in English, six (6) issues a year with the coverage of: Food Science and Technology Nutrition and Dietetics Agriculture, multidisciplinary Chemistry, multidisciplinary The scope of the Journal includes: Food Science, Food Technology and Food Biotechnology Product Development and Sensory Evaluation Food Habits, Nutrition, and Health Food Safety and Quality Food Chemistry, Food Microbiology, Food Analysis and Testing Food Engineering Food Packaging Food Waste Management Food Entrepreneur Food Regulatory Post-Harvest Food Management Food Supply Chain Management Halal Food and Management
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