Characterization of α-Cellulose from Bagasse Cane Bz 132 (Saccharum officinarum)

T. R. Hidayani, B. Wirjosentono, D. Nasution, Tamrin
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Abstract

: A study concerning the separation of α - cellulose from bagasse were conducted using Okhamafe. The first stage is the preparation of bagasse powder type Bz 132. Stage second is the separation of α - cellulose from bagasse is done with the method Okhamafe done by immersion in 3.5 % HNO acid, bleaching with Sodium Hypochlorite 1.75 % and purification with 17.5 % NaOH. The third stage is the characterization of α cellulose from bagasse types Bz 132 showed visible surface with large round -shaped grains are almost the same size (uniform). This may indicate that the resulting α - cellulose has a form of homogeneous size (as large). From the analysis of functional groups with the free OH groups visible wave number 4001.50 cm-1 which shows a typical chain of cellulose CH2OH and OH hydrogen bonds with wave number 3437.30 cm-1 as supporting data. Of the thermal test with test results obtained DTA melting point at a temperature of 60oC and 320oC decomposition point.
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甘蔗渣Bz 132 (Saccharum officinarum) α-纤维素的表征
采用Okhamafe对甘蔗渣中α -纤维素进行了分离研究。第一阶段是制备bz132型甘蔗渣粉末。第二阶段采用Okhamafe法分离甘蔗渣中的α -纤维素,方法为3.5% HNO酸浸泡,1.75%次氯酸钠漂白,17.5% NaOH纯化。第三阶段是对甘蔗渣型α纤维素的表征,bz132型α纤维素表面有较大的圆形颗粒,颗粒大小几乎相同(均匀)。这可能表明所得到的α -纤维素具有均匀尺寸的形式(同样大)。通过对游离OH官能团的可见波数4001.50 cm-1的分析,得到了典型的纤维素CH2OH链和波数3437.30 cm-1的OH氢键作为支持数据。对热试验用试验结果得出了DTA在温度为60oC时的熔点和320oC时的分解点。
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