Magnesium Impregnated Silica Mesoporous Prepared using Ester Ricinoleic as Template for the Esterification

Andriayani, Marpongahtun, Y. Muis
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Abstract

: Synthesis of mesoporous silica material was carried out using ricinoleate ester as a template. Mesoporous silica products were characterized using FT-IR, XRD, SEM and nitrogen adsorption. Mesoporous silica material was impregnated with magnesium nitrate, impregnation products were characterized using FT-IR, XRD, SEM and BET analysis. MgO impregnated silica mesoporous is applied as a catalyst in the reaction of esterification of castor oil to ricinoleate ester.
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以蓖麻油酸酯为模板剂制备镁浸渍二氧化硅介孔酯化反应
以蓖麻油酸酯为模板,合成了介孔二氧化硅材料。采用红外光谱(FT-IR)、x射线衍射(XRD)、扫描电镜(SEM)和氮气吸附等方法对介孔二氧化硅产品进行了表征。采用硝酸镁对介孔二氧化硅材料进行浸渍,浸渍产物采用FT-IR、XRD、SEM和BET分析进行表征。以MgO浸渍二氧化硅介孔为催化剂,研究了蓖麻油酯化制蓖麻油酸酯的反应。
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