Structural analysis of Cu-based FeCr reinforced composites prepared by mechanical alloying

S. Yilmaz, T. Teker, S. Aydin
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Abstract

Abstract Production and structural investigations of Cu-based FeCr reinforced composite were performed by using mechanical alloying, optical microscope, scanning electron microscope, X-ray diffraction and hardness test. The increment in FeCr addition caused the increment in the cold deformation rate. This situation resulted in breakage of the powder particles throughout mechanical alloying. Thus, the grain dimension of the FeCr powders decreased and the Fe wt.% in the CuCr powders advanced. The collision force between the Cu-Cr powder and the grinding ball weakened with the increase of FeCr concentration and resulted as higher reinforcement size. After mechanical milling, FeCr grains decreased in size more than copper grains due to the ductility of copper grains. The smaller crystals occurred after grinding, and increased the grain boundary zone for further spread of Cr into the Cu. Despite the high sintering process, the high sintering temperature improved the compactness of the alloys, but caused coarsening of the nanoparticles. The mechanical alloying time, reinforcement wt.% and sinter temperature were effective on the micro-hardness of the microstructure.
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机械合金化制备cu基FeCr增强复合材料的结构分析
采用机械合金化、光学显微镜、扫描电镜、x射线衍射和硬度测试等方法对cu基FeCr增强复合材料的制备和组织进行了研究。FeCr添加量的增加导致冷变形速率的增加。这种情况导致粉末颗粒在机械合金化过程中断裂。因此,FeCr粉末的晶粒尺寸减小,CuCr粉末中的Fe wt.%提高。随着FeCr浓度的增加,Cu-Cr粉末与磨球之间的碰撞力减弱,增强尺寸增大。机械铣削后,由于铜晶粒的延展性,铁铁晶粒的尺寸减小幅度大于铜晶粒。磨后晶粒变小,晶界区增大,使Cr进一步向Cu扩散。高烧结温度虽然提高了合金的致密性,但却导致纳米颗粒的粗化。机械合金化时间、增强剂wt.%和烧结温度对显微组织的显微硬度有影响。
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