Shrinkage Kinetics during Sintering W-Ni-Fe Heavy Alloy with Ultrafine Grain

Wang Jun, Z. Liying, G. Zhimeng, Lin Tao, Wu Chengyi, Wu Qinghua
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引用次数: 3

Abstract

The characteristics of swell-shrinkage kinetic curve during sintering the compact of W-Ni- Fe 10% with primary mean grain size less than 200 nm in hydrogen atmosphere was researched by high tem- perature dilatometer. And the effects of the average size of tungsten particle and green density on shrinkage commence temperature, sharp shrinkage temperature and shrinkage rate were also studied. It shows that shrink age commence temperature and sharp shrinkage temperature of the compact with ultrafine grain are 970℃ and 1240 ℃ respectively. The maximum shrinkage rate is 9 μm/℃. The shrinkage ratio decreases with the increase of green density and increases with the increase of sintering temperature.
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超细晶W-Ni-Fe重合金烧结收缩动力学
采用高温膨胀仪研究了10% W-Ni- Fe合金初次平均晶粒尺寸小于200nm在氢气气氛中烧结时的膨胀-收缩动力学曲线特征。研究了钨的平均粒径和生坯密度对收缩开始温度、急剧收缩温度和收缩率的影响。结果表明:超细晶粒致密材料的收缩时效开始温度为970℃,急剧收缩温度为1240℃;最大收缩率为9 μm/℃。收缩率随生坯密度的增加而减小,随烧结温度的升高而增大。
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