Characterization of Silica Nanoparticles from Pumice as an Aerogel Adsorbent

Rahma Hidayah, D. Kurniawati, Alizar Alizar
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Abstract

Pumice is often found around the banks of rivers, this stone is a type of igneous rock formed from volcanic eruptions. One of the compounds contained in pumice is silica. Therefore, the synthesis of silica nanoparticles from pumice using the sol gel method was used because it is simpler and more efficient in terms of cost and processing time. the initial step was by reacting pumice powder and NaOH at 70°C - 80°C then synthesized by adding 2M HCI to form a gel or white precipitate, soaking in ethanol, teos, hexane solutions was then synthesized to become an aerogel. Silica synthesis results into silica aerogels were characterized by FTIR and XRF. From FTIR silanol and siloxane functional groups were found, and the SiO2 composition increased to 93,299% after synthesis.
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浮石二氧化硅纳米颗粒作为气凝胶吸附剂的表征
浮石经常在河岸周围发现,这种石头是一种由火山喷发形成的火成岩。浮石中含有的一种化合物是二氧化硅。因此,采用溶胶-凝胶法从浮石中合成二氧化硅纳米颗粒,因为它在成本和处理时间方面更简单,效率更高。初始步骤是浮石粉与NaOH在70℃- 80℃下反应,然后加入2M HCI合成,形成凝胶或白色沉淀,在乙醇、正己烷溶液中浸泡,然后合成成气凝胶。用FTIR和XRF对二氧化硅气凝胶的合成结果进行了表征。从红外光谱中发现了硅醇和硅氧烷官能团,合成后SiO2含量提高到93,299%。
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