Rapid synthesis of carbon nanotubes by bulk and localized inductive heating

B. D. Sosnowchik, Liwei Lin
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引用次数: 7

Abstract

In this work, we report a rapid yet simple methodology for the synthesis of carbon nanotubes (CNTs) in a room temperature environment using an inductive heating system with either a) bulk synthesis on silicon chips, or b) local synthesis on suspended MEMS structures. This setup enables growth and integration of CNTs with MEMS structures in a matter of 1-2 minutes. For bulk synthesis, high growth rates of up to 200 mum/min were obtained, resulting in growth of vertically aligned CNTs with an average diameter of 6.8nm. Integration from bulk- grown CNTs on MEMS structures resulted in lower resistances from larger diameter CNTs. Localized synthesis and integration was also obtained on suspended copper microstructures, illustrating an ohmic CNT response with a resistance of 110 kOmega. The breadth of synthesis and integration capabilities enabled by inductive heating illustrates a new class of rapid synthesis for vapor-liquid-solid-grown nanostructures.
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本体和局部感应加热快速合成碳纳米管
在这项工作中,我们报告了一种在室温环境下使用感应加热系统快速而简单地合成碳纳米管(CNTs)的方法,其中a)硅片上的整体合成或b)悬浮MEMS结构上的局部合成。这种设置可以在1-2分钟内实现碳纳米管与MEMS结构的生长和集成。对于体合成,获得了高达200 mum/min的高生长速率,从而生长出平均直径为6.8nm的垂直排列的碳纳米管。大块生长的碳纳米管在MEMS结构上的集成导致更大直径碳纳米管的电阻更低。在悬浮铜微结构上也获得了局部合成和集成,说明了电阻为110 kOmega的欧姆碳纳米管响应。通过感应加热实现的合成和集成能力的广度说明了一种新型的蒸汽-液体-固体生长纳米结构的快速合成。
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