Suppression of Mg Propagate into Subsequent Layers by Furnace Annealing

Wenxin Tang, L. Zhang, Xing Wei, Jiaan Zhou, Weining Liu, Zengli Huang, Guohao Yu, Baoshun Zhang
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Abstract

Multilayers and trench MOS structures have been involved to investigate the diffusion behavior of Mg atoms and the corresponded electrical properties. Four groups of p-n + stacked layers were grown to study the effect of different interfacial treatment. The growth conditions of these four groups were identical except for different interfacial treatment during the growth, including as grown, furnace annealing, AlGaN interlayer and furnace annealing with AlGaN interlayer. Furnace annealing refers to 850°C for 10 min in a nitrogen atmosphere in MOCVD and AlGaN interlayer means a 50 nm Si-doped $\text{Al}_{0.08}\text{Ga}_{0.92}\mathrm{N}$ layers have been inserted. The slope of the Mg concentration for the furnace annealing sample is 90 s/dec-less than 63% of the as-grown sample. SIMS results also reveals that furnace annealing introduce an interface with a low conductivity while an improved sheet resistance of subsequent n + layer from 630 Ω/Ÿ to 415 Ω/Ÿ. Especially, the sum of resistance, including the drain and source contact resistance, contact layer resistance (RS and RD) and channel resistance (RCH), decreased from 151.5 Ω.mm to 125.9 Ω.mm via furnace annealing which has been verified by quasi-vertical n+-p-unintentionally doped (n+-p-uid) GaN-on-GaN trench MOS structure with different trench width. Furnace annealing has been successfully used to prevent Mg atoms from Metalorganic Chemical Vapor Deposition (MOCVD) grown p-GaN:Mg layers riding into subsequently deposited n+-type layer and improve the electrical characteristic of sheet resistance and ON-resistance in the device of trench MOS structure. This work shows a great reference value for GaN with a buried p-GaN structure.
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炉内退火法抑制Mg向后续层的扩散
利用多层和沟槽MOS结构研究了Mg原子的扩散行为和相应的电学性质。培养了四组p-n +堆叠层,研究了不同界面处理的效果。四组的生长条件基本相同,只是生长过程中的界面处理不同,包括生长、炉退火、AlGaN中间层和带AlGaN中间层的炉退火。炉退火是指在MOCVD的氮气气氛中850℃退火10 min, AlGaN中间层是指插入50 nm si掺杂的$\text{Al}_{0.08}\text{Ga}_{0.92}\ maththrm {N}$层。炉后退火样品的Mg浓度斜率为90 s/dec,小于生长样品的63%。SIMS结果还表明,炉内退火导致界面电导率较低,而后续n +层的片材电阻从630 Ω/Ÿ提高到415 Ω/Ÿ。特别是漏极和源极接触电阻、接触层电阻(RS和RD)和通道电阻(RCH)之和从151.5 Ω开始减小。Mm到125.9 Ω。通过不同沟槽宽度的准垂直n+-p掺杂(n+-p-uid) GaN-on-GaN沟槽MOS结构验证了该方法的有效性。采用炉内退火技术成功地防止了金属有机化学气相沉积(MOCVD)生长的p-GaN:Mg层中的Mg原子进入随后沉积的n+型层,并改善了沟槽MOS结构器件的片电阻和on电阻的电学特性。本研究对具有埋藏p-GaN结构的GaN具有重要的参考价值。
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