Development of new micro gas preconcentrator using novel electroless gold plating process

Chun-Yen Kuo, P.-S Chen, K. Chiu, C.-J. Lu, W. Tian
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Abstract

This article presents a novel electroless gold plating method to fabricate a thin film heater for a new micro preconcentrator (μPCT) utilized in a micro gas chromatograph (μGC). The gold thin film utilized for heating with a high porosity is fabricated within the surface of the μPCT channel. The μPCT can be heated to >300°C repeatedly by applying a constant electrical power. A commercial Tenax TA was used as an adsorbent. Four volatile organic compounds (VOCs), acetone, benzene, toluene and m-xylene, are successfully collected and concentrated with the narrow peak width at half height (PWHH) (1.92 to 3.88 s). Compared to our previous results, this study presents up to approximately 49% narrower PWHH and approximately six times faster heating.
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新型化学镀金微型气体预选厂的研制
本文提出了一种新型化学镀金方法,用于制备微气相色谱仪(μGC)中新型微预富集器(μPCT)的薄膜加热器。在μPCT通道表面制备了用于加热的高孔隙率金薄膜。μPCT可以通过恒定的功率反复加热到>300℃。采用商用Tenax TA作为吸附剂。四种挥发性有机化合物(VOCs),丙酮,苯,甲苯和间二甲苯,在半高峰宽(1.92至3.88 s)的情况下成功地收集和浓缩,与我们之前的结果相比,本研究的PWHH缩小了约49%,加热速度提高了约6倍。
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