Exploring the Effect of Operational Factors and Characterization Imperative to the Synthesis of Silver Nanoparticles

Silver Nanoparticles - Fabrication, Characterization and Applications Pub Date : 2018-07-18 DOI:10.5772/INTECHOPEN.76947

A. O. Dada, F. A. Adekola, O. Adeyemi, O. Bello, C. Adetunji, O. J. Awakan, A. G. Femi-Adepoju

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引用次数: 21

Abstract

The synthesis and application of silver nanoparticles are increasingly becoming attractive. Hence, a critical examination of the various factors needed for the synthesis of silver nanoparticles as well as the characterization is imperative. In light of this, we addressed in this chapter, the nitty-gritty on the operational parameters (factors) and characterization relevant to synthesis of silver nanoparticle. The following characterization protocols were discussed in the context of silver nanoparticle synthesis. These protocols include spectroscopic techniques such as ultraviolet visible spectroscopy (UV–Vis), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy-dispersive X-ray spectroscopy (EDX), X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TGA) and X-ray photoelectron spectroscopy (XPS). Keywords: silver nanoparticles, characterization, morphology, operational factors

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探索操作因素和表征对银纳米粒子合成的影响

纳米银的合成和应用越来越受到人们的关注。因此，对银纳米颗粒合成和表征所需的各种因素进行严格检查是必要的。鉴于此，我们在本章中讨论了与银纳米颗粒合成相关的操作参数(因素)和表征的本质。在纳米银合成的背景下，讨论了以下表征方案。这些协议包括光谱技术，如紫外可见光谱(UV-Vis)、傅里叶变换红外光谱(FTIR)、扫描电子显微镜(SEM)、透射电子显微镜(TEM)、能量色散x射线光谱(EDX)、x射线荧光(XRF)、x射线衍射(XRD)、热重分析(TGA)和x射线光电子能谱(XPS)。关键词:纳米银，表征，形貌，操作因素

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Silver Nanoparticles - Fabrication, Characterization and Applications

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