Method Development for Analysis of Essential Oils Authenticity using Gas Chromatography-Mass Spectrometry (GC-MS)

N. N. Aidha, R. Yunilawati, Irma Rumondang
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引用次数: 1

Abstract

Essential oils widely used as fragrances and flavours in the food and cosmetics industry and also for the medical and pharmaceutical fields for various effects. The demand increasing of essential oil caused the cases of adulteration that affect the authenticity of essential oil. The authenticity is important in ensuring the quality of essential oil. This study was aimed to analyse the authenticity of essential oil use Gas ChromatographyMass Spectrometry (GC-MS) by determining its chemical component. The experiment included repeatability, accuracy, and limit of detection. GC performed on HP-5MS capillary column operated in 600C-2400C temperature programs. This method successfully applied to all types of essential oil with limit detection of clove oil was 0.02 ppm, citronella oil was 0.033 ppm, patchouli oil was 0.005 ppm, and lemongrass was 0.016 ppm. All types of essential oil also have good repeatability and accuracy with these methods. This study will facilitate the scientific community by enhancing the efficient method for essential oil.
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气相色谱-质谱联用分析精油真伪方法的建立
精油广泛用于食品和化妆品行业的香料和香精,也用于医疗和制药领域的各种效果。随着市场对精油需求量的增加,精油掺假事件不断发生,影响了精油的真伪。精油的真实性是保证精油质量的重要因素。本研究采用气相色谱-质谱联用技术测定精油的化学成分,分析其真伪。实验包括重复性、准确性和检出限。GC在HP-5MS毛细管柱上进行,操作温度为600 -2400℃。该方法适用于各类精油,丁香油的检出限为0.02 ppm,香茅油的检出限为0.033 ppm,广藿香油的检出限为0.005 ppm,柠檬草的检出限为0.016 ppm。所有类型的精油也具有良好的重复性和准确性。本研究将通过提高精油的有效方法为科学界提供便利。
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