Kinetics Study of LiFePO4 Synthesis Reaction with Solid State Method

E. Dyartanti, A. R. Nurohmah, I. P. Lestari, M. I. Putra, S. S. Nisa, Ulfa Pratiwi
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Abstract

Lithium Ferro Phosphate (LiFePO4) is a cathode that has the advantage of abundant raw material, inexpensive and easily upgraded compared to other cathode. The method commonly used for LiFePO4 synthesis is solid state. It is important to study kinetics in this process for product optimization. There are two methods in determining the kinetics of product formation including Thermogravimetric Differential Thermal Analysis (TG-DTA) and X-ray Diffraction (XRD). Meanwhile, Cyclic Voltammetry (CV) and Electrochemical Impedance Spectroscopy (EIS). Meanwhile, CV and EIS were used to determine electrochemical kinetics.
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固相法合成LiFePO4反应动力学研究
磷酸铁锂(LiFePO4)是一种原料丰富、价格低廉、易于升级的正极材料。合成LiFePO4常用的方法是固态法。研究这一过程的动力学对产品优化具有重要意义。测定产物形成动力学的方法有热重差热分析(TG-DTA)和x射线衍射(XRD)两种。循环伏安法(CV)和电化学阻抗谱法(EIS)。同时,利用CV和EIS测定了电化学动力学。
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