Microstructure development and mechanical behaviour of pure copper processed by the novel TWO-CAP procedure

IF 2.4 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Testing Pub Date : 2023-06-23 DOI:10.1515/mt-2023-0011
H. Kaya, M. Uçar, Mehmet Şahbaz, A. Kentli, Kerim Özbeyaz, Serkan Öğüt
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Abstract

Abstract In this study, thin-walled open channel angular pressing (TWO-CAP) technique was applied to pure copper specimens as a novel severe plastic deformation (SPD) method. The TWO-CAP process was applied to the specimens up to four passes. After each pass, the microstructural and mechanical characterization of the material was investigated by tensile and hardness tests along with OM, SEM, EDS, TEM and XRD analyses. As a result, a highly increase in the mechanical properties was obtained, in addition satisfactory grain refinement was observed in microstructures. Strength and hardness values were positively affected from the minimizing the grain sizes after TWO-CAP process. Another reason of the improvements in mechanical properties can be explained as the increase in dislocation density. Furthermore, the effect of the TWO-CAP process on the dislocation density of the material has been demonstrated by XRD and TEM analyses in nanoscale. Moreover, the strain equation has been developed analytically and the effect of each pass on strain was calculated. Finally, the effect of the process on the stress-strain properties of the material was examined by the numerical analysis method and the study was verified.
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新型TWO-CAP工艺处理纯铜的微观组织发展和力学行为
摘要本研究将薄壁开槽角压(TWO-CAP)技术作为一种新型的严重塑性变形(SPD)方法应用于纯铜试样。2 - cap工艺应用于样品多达四次。每道次后,通过拉伸和硬度测试以及OM、SEM、EDS、TEM和XRD分析对材料的微观组织和力学特性进行了研究。结果表明,合金的力学性能得到了显著提高,显微组织也得到了令人满意的晶粒细化。通过减小晶粒尺寸对强度和硬度值产生积极影响。力学性能改善的另一个原因可以解释为位错密度的增加。此外,通过XRD和TEM分析,在纳米尺度上证实了TWO-CAP工艺对材料位错密度的影响。推导了应变方程,并计算了各道次对应变的影响。最后,采用数值分析方法考察了工艺对材料应力应变性能的影响,并对研究结果进行了验证。
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来源期刊
Materials Testing
Materials Testing 工程技术-材料科学:表征与测试
CiteScore
4.20
自引率
36.00%
发文量
165
审稿时长
4-8 weeks
期刊介绍: Materials Testing is a SCI-listed English language journal dealing with all aspects of material and component testing with a special focus on transfer between laboratory research into industrial application. The journal provides first-hand information on non-destructive, destructive, optical, physical and chemical test procedures. It contains exclusive articles which are peer-reviewed applying respectively high international quality criterions.
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