Making Composites from Mixing Limestone with Addition of Latex

A. Siregar, S. Gea, Nora Indriani
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Abstract

: Research on mixing of limestone with the addition of latex in making composites have been done. This study uses limestone originating from Sidikalang where crushed limestone using ball mill then calcined at 900 o C for 2 hours then tested using XRD Pan Analytical X’pert Powder PW 30/40 to determine the presence of CaO compounds with the greatest intensity of 3036 at θ =37.3556 and particle size tested using PSA Shimadzu SALD-2300 is obtained an average of 731.7 nm. Then limestone powder (LSP) is used as a filler with various variations on latex composites. Analyzing of the morphology using SEM FEI Inspect-S50 can be seen from the photo that limestone powder can be evenly distributed on compsites 800 g of latex + 200 g of limestone powder while in the next variation the limestone powder is not evenly distributed because the addition of the filler increases but the addition of the matrix decreases. The mechanical properties of latex composites with limestone powder were tested using ASTM D-412 where optimum tensile strength was found in 800 g of latex + 200 g of limestone powder is 1.279 MPa and optimum elongation of 1000 g latex is 4.328 mm/mm. Thermal properties were tested using TGA ASTM E1131 obtained by decomposition thermal at 300-400 o C because in the sample 1000 g of latex has thermal stability at 377.39 o C and in the sample 800 g of latex + 200 g of limestone powder has thermal stability at 378.21 o C.
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石灰石掺加乳胶制备复合材料
对石灰石与乳胶的掺合制备复合材料进行了研究。本研究使用的石灰石来自Sidikalang,石灰石经过球磨机粉碎,900℃下煅烧2小时,然后使用XRD Pan Analytical X 'pert Powder PW 30/40进行测试,以确定CaO化合物的存在,其最大强度为3036,θ =37.3556,使用PSA Shimadzu SALD-2300测试的粒度平均为731.7 nm。然后用石灰石粉末(LSP)作为填料,在乳胶复合材料上进行各种变化。利用SEM FEI Inspect-S50对其形貌进行分析,从照片中可以看出,当乳胶量为800 g +石灰石粉为200 g时,石灰石粉在复合材料上的分布较为均匀,而下一个变化中,由于填料的添加量增加而基体的添加量减少,石灰石粉的分布并不均匀。采用ASTM D-412测试了石灰石粉乳胶复合材料的力学性能,其中800g乳胶+ 200g石灰石粉的最佳抗拉强度为1.279 MPa, 1000g乳胶的最佳伸长率为4.328 mm/mm。热性能测试使用在300-400℃分解热得到的TGA ASTM E1131,因为样品中1000g乳胶在377.39℃时具有热稳定性,样品中800g乳胶+ 200g石灰石粉末在378.21℃时具有热稳定性。
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