Synthesis, structure and morphology of composites based on magnesium ferrite and carbon nitride

A. Ivanets
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引用次数: 1

Abstract

The composites based on magnesium ferrite and carbon nitride were synthesized by the sol-gel method in combination with thermochemical condensation. The effect of the synthesis method on the crystalline structure, the phase and chemical composition, and the morphology of composites was studied by the X-ray diffraction, IR spectroscopy, scanning electron microscopy, and energy-dispersive X-ray spectroscopy techniques. It was found that, depending on the conditions of the sol-gel stages, the initiation of self-combustion high-temperature synthesis and melanin thermochemical condensation, composites with different crystalline structure and morphology were prepared. The obtained results are important for the development of the heterogeneous Fenton- and photo-Fenton catalysts based on magnesium ferrite and carbon nitride composites.
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铁素体镁与氮化碳复合材料的合成、结构与形貌
采用溶胶-凝胶法结合热化学缩合法制备了铁酸镁与氮化碳复合材料。采用x射线衍射、红外光谱、扫描电镜和能量色散x射线能谱技术研究了合成方法对复合材料晶体结构、物相、化学成分和形貌的影响。研究发现,根据溶胶-凝胶阶段、自燃高温合成起始和黑色素热化学缩合的不同条件,可以制备出不同晶体结构和形态的复合材料。所得结果对开发基于铁酸镁-氮化碳复合材料的非均相Fenton和光Fenton催化剂具有重要意义。
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