XRD, dielectric and magnetic studies of Cd2Nb2O7 ceramics obtained from mechano-synthesized nanopowders

M. Połomska, B. Hilczer, Ewa Markiewicz, Zbigniew Trybuła, Bartłomiej Andrzejewski, I. S. Wiza, Adam Pietraszko
{"title":"XRD, dielectric and magnetic studies of Cd2Nb2O7 ceramics obtained from mechano-synthesized nanopowders","authors":"M. Połomska, B. Hilczer, Ewa Markiewicz, Zbigniew Trybuła, Bartłomiej Andrzejewski, I. S. Wiza, Adam Pietraszko","doi":"10.1109/ISAF.2012.6297742","DOIUrl":null,"url":null,"abstract":"Dielectric response, thermal and magnetic properties of hot-pressed ceramics obtained from Cd2Nb2O7 nanopowders synthesized by high-energy milling of CdO and Nb2O5 were studied. The transition from cubic to orthorhombic phase was found to be shifted downwards by ~50 K in comparison with that reported for single crystals. Below 150 K four relaxation processes were revealed and characterized. A broad specific heat anomaly with maximum at 18K, similar to that reported for single crystals was observed. Small magnetic hysteresis loop observed for the ceramics at 4 K can be due to defects introduced in the process of mechanical synthesis.","PeriodicalId":20497,"journal":{"name":"Proceedings of ISAF-ECAPD-PFM 2012","volume":"29 1","pages":"1-4"},"PeriodicalIF":0.0000,"publicationDate":"2012-07-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Proceedings of ISAF-ECAPD-PFM 2012","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/ISAF.2012.6297742","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

Abstract

Dielectric response, thermal and magnetic properties of hot-pressed ceramics obtained from Cd2Nb2O7 nanopowders synthesized by high-energy milling of CdO and Nb2O5 were studied. The transition from cubic to orthorhombic phase was found to be shifted downwards by ~50 K in comparison with that reported for single crystals. Below 150 K four relaxation processes were revealed and characterized. A broad specific heat anomaly with maximum at 18K, similar to that reported for single crystals was observed. Small magnetic hysteresis loop observed for the ceramics at 4 K can be due to defects introduced in the process of mechanical synthesis.
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
机械合成纳米粉末制备的Cd2Nb2O7陶瓷的XRD、介电和磁性研究
研究了CdO和Nb2O5高能研磨法制备的Cd2Nb2O7纳米粉体热压陶瓷的介电响应、热性能和磁性能。与单晶相比,发现从立方相到正交相的转变向下移动了~50 K。在150k以下发现并表征了四个弛豫过程。在18K处观察到广泛的比热异常,最大比热异常与单晶相似。在4k时,陶瓷的磁滞回线很小,这可能是由于机械合成过程中引入的缺陷。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Dielectric and piezoelectric properties of modified (Na, K)NbO3 ceramics substituted with KNbO3 Vibrational fingerprints of LiNbO3-LiTaO3 mixed crystals Fe valence determination in doped SrTiO3 epitaxial films Role of interfaces in nanostructured CoFe2O4 films An investigation into the electrical properties of doped barium titanate using EIS
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1