Development of the Chemical Experiment Device of Promoting the Reversible Reaction

Zhou Xiong, Wu Xinping, Qin Honglian
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Abstract

The chemical experiment device which can promote the reversible reaction has been introduced that combined with the preparative experiment of acetidin by the Le chateliers principle. The device referenced the industrial production method-reaction distillation method. It includes the dephlegmator, water separator, reflux device, and so on. The ester and the water can be steamed out of the system continuously, so it can promote the balance. Through the practice application, the product is less impurity, the subsequent refined is easy, the yield is higher. The experiment teaching effect is improved by the use of the device.
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促进可逆反应化学实验装置的研制
结合利用勒夏特列原理制备乙酸乙酯的实验,介绍了促进可逆反应的化学实验装置。该装置参考了工业生产方法-反应精馏法。包括除痰器、水分离器、回流装置等。酯和水可以连续蒸出系统,因此可以促进平衡。经实际应用,所得产品杂质少,后续精制容易,收率较高。该装置的使用提高了实验教学效果。
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来源期刊
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期刊介绍: "Experiment Science and Technology" is a comprehensive journal of natural sciences and engineering sponsored by the Sichuan Provincial Department of Education and the University of Electronic Science and Technology of China and the Sichuan Higher Education Association. It aims to report the development status, achievements or interim achievements of scientific research in natural sciences with talent training as the center; exchange research results and experience in the design, development, function development, maintenance management and supply management of instruments and technical equipment; explore common problems in the construction of laboratories at all levels and types, team building and improving the efficiency of instrument use from a technical perspective; explore new ideas, new ways and new measures for experimental teaching reform and innovation. The journal mainly has columns such as experimental technology, experimental teaching and teaching experiments, virtual simulation technology, laboratory environment and safety, experimental instrument development and maintenance, laboratory construction and management, and large-scale instrument management and sharing.
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