Eugenol Production from Clove Oil in Pilot Plant Scale for Small and Medium Enterprises (SME)

A. Nurdin
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Abstract

: Clove oil was the largest essential oil commodity in Indonesia and production at Small and Medium Enterprises (SME) was still below the standard quality due to low eugenol levels (70-80%). The eugenol level can be increased by isolation which generally can be carried out by saponification and neutralization methods. This method was the most widely used, inexpensive, and easy to scale-up from the laboratory scale to the pilot plant scale. In this research, the production of eugenol from clove oil has been carried out in a pilot plant scale with stages of saponification reaction using sodium hydroxide and neutralization using sulfuric acid followed by vacuum distillation. All stages of this process produce eugenol with a yield of 50.25%, and an increase in eugenol levels from 75% to 98%. The eugenol production technology that has been carried out was expected to provide a solution for the small clove oil industry to improve its quality.
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中小企业丁香油中试生产丁香酚
丁香油是印度尼西亚最大的精油商品,由于丁香酚含量低(70-80%),中小型企业(SME)的生产仍低于标准质量。丁香酚的含量可以通过分离来提高,这种分离通常可以通过皂化和中和方法来实现。该方法应用最广泛,价格低廉,易于从实验室规模扩大到中试工厂规模。以丁香油为原料,采用氢氧化钠皂化、硫酸中和、真空蒸馏的中试工艺生产丁香酚。该工艺各阶段的丁香酚产率均为50.25%,丁香酚含量由75%提高到98%。所开展的丁香酚生产技术有望为小丁香油行业提高丁香油质量提供一种解决方案。
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