Method and apparatus for automatic high-throughput synthesis of energetic salts

Qiuxiao Wang, Tao Wang, Yifei Zhou, Haixiang Gao
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Abstract

Energetic materials can instantly combust and release a large amount of energy in responding external impulses. Due to its energy characteristics, it has a wide range of practical applications: military and civilian. Designing high-energy-density materials with better performance, lower sensitivity, and more environmental friendliness has become a hotspot in the field of energetic materials in recent years. Energetic salts are formed by acid-base or metathesis reactions of different types of anions and cations. Energetic salts are a new class of energetic materials which were developed in recent years. Usually, they have high nitrogen content, high enthalpy of formation, high detonation performance, are relative stable to external stimuli, and have a wide range of application prospects in the fields of new explosives: low characteristic signal propellants, gas generators, low smoke or smokeless pyrotechnics. The synthesis method of energetic salts is simple, and the types of energetic materials are greatly enriched. This research takes energetic salts as the synthesis target and adopts multi-channel automation technology for high-throughput synthesis, which can improve the efficiency, reduce labor costs, and greatly increase the synthesis speed, which is of great significance for accelerating the synthesis of new energetic salts.
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一种自动高通量合成含能盐的方法和装置
高能材料可以瞬间燃烧,并在响应外部脉冲时释放大量能量。由于其能量特性,它具有广泛的实际应用:军用和民用。设计性能更好、灵敏度更低、更环保的高能量密度材料已成为近年来含能材料领域的研究热点。含能盐是由不同类型的阴离子和阳离子的酸碱或复分解反应形成的。含能盐是近年来发展起来的一类新型含能材料。通常具有含氮量高、生成焓高、爆轰性能好、对外部刺激相对稳定等特点,在低特征信号推进剂、气体发生器、低烟或无烟烟火等新型炸药领域具有广泛的应用前景。含能盐的合成方法简单,含能材料种类丰富。本研究以含能盐为合成靶点,采用多通道自动化技术进行高通量合成,可以提高效率,降低人工成本,大大提高合成速度,对于加快新型含能盐的合成具有重要意义。
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