Growth and characterization of pure and L-Glutamic acid doped zinc tris(thiourea) sulphate (ZTS) single crystals

B. S. Samuel, R. Rajasekaran
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Abstract

Single crystals of pure and L-glutamic acid doped zinc tris (thiourea) sulphate(ZTS) were grown from aqueous solution by slow evaporation technique. The grown crystals were subjected to various studies such as FTIR, Powder X-Ray diffraction, second harmonic generation (SHG), UV-visible spectra and thermal analysis (TG-DTA). The FTIR study confirms the incorporation of L- glutamic acid into ZTS crystal. The enhancement of SHG efficiency was observed in doped ZTS crystal. The doped crystals are optically transparent and thermally stable.
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纯和l -谷氨酸掺杂的三硫脲硫酸锌(ZTS)单晶的生长和表征
采用慢蒸发法制备了纯和l -谷氨酸掺杂的三硫脲硫酸锌(ZTS)单晶。对生长的晶体进行了FTIR、粉末x射线衍射、二次谐波产生(SHG)、紫外可见光谱和热分析(TG-DTA)等研究。FTIR研究证实了L-谷氨酸在ZTS晶体中的掺入。在掺杂ZTS晶体中观察到SHG效率的提高。掺杂晶体具有光学透明性和热稳定性。
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