从棕榈油空颗粒中分离纳米纤维素,使用酸性水解作为生物医学材料

Ayu Syufiatun Br Tarigan
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引用次数: 0

摘要

采用酸水解法从油棕空果串(OPEFB)中分离纳米纤维素。用10%盐酸水解2小时,然后离心、超声和半透膜透析。利用FT-IR对所得结果进行了测试,发现在3000 ~ 3500 cm-1波数范围内存在一个-OH官能团,在2850 ~ 3000 cm-1范围内存在一个C-H基团,在1330 ~ 1465 cm-1波数范围内存在-CH2弯曲,在1000 ~ 1100 cm-1波数范围内存在CO基团。这表明该产品以纤维素的形式存在。用PSA(粒度分析仪)测定了纤维素的粒径分布,得到的纳米纤维素粒径约为7.2 nm。
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ISOLASI NANOSELULOSA DARI TANDAN KOSONG SAWIT MENGGUNAKAN HIDROLISIS ASAM SEBAGAI MATERIAL BIOMEDIS
This study aims to isolate nanocellulose from oil palm emptry fruit bunches (OPEFB) using acid hydrolysis method. Hydrolysis was carried out for 2 hours using 10% HCl and followed by centrifugation, ultrasonication and dialysis using a semipermeable membrane. The results obtained were tested by FT-IR, and it was found that there was a -OH functional group at a wavenumber between 3000-3500 cm-1, a C-H group in the area 2850-3000 cm-1, -CH2 bending at a wavenumber 1330-1465 cm-1 and the CO group at wave numbers 1000-1100 cm-1. This indicates that the product is in the form of cellulose. The particle size distribution of cellulose was tested with a PSA (Particle Size Analyzer) and the nanocellulose was about 7.2 nm in size.
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