电弧离子镀法制备氮化铬涂层的粘接性能评价

R. Murakami, Yun-Hae Kim, Kazushi Kimura, D. Yonekura, Do-Hoon Shin
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引用次数: 3

摘要

通过划痕试验和销盘磨损试验来阐明CrN涂层的开裂和脱层行为。采用电弧离子镀方法将CrN薄膜涂覆在JIS A2024铝合金基体上。通过改变沉积过程中的偏置电压,制备了8种单层和多层涂层。LCI和LCII值不随层数的增加而提高。单层膜的临界载荷随偏压的增加而减小。结果表明,对于多层涂层,偏置电压的组合影响临界载荷。临界载荷在很大程度上取决于动态硬度和杨氏模量。特别是,多层涂层的临界载荷受中间层和底层性能以及顶层表面粗糙度、硬度和杨氏模量的影响。在高偏置电压下沉积的单层涂层在针盘式磨损试验中,即使单层涂层的临界载荷高于多层涂层的临界载荷,也会发生大面积的薄膜分层。如果脆性的顶层可以通过滑动接触被破坏和分层,那么在0V的偏置电压下涂覆的韧性底层可以承受薄膜的完全分层。
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Evaluation of Adhesive Behaviors of Chromium Nitride Coating Films Produced by Arc Ion Plating Method
Scratch tests and pin-on-disk wear tests were performed to clarify the cracking and delaminating behavior of CrN coatings. The CrN films were coated onto an aluminum alloy substrate, JIS A2024, by an arc ion plating method. Eight types of single-layered coating and multilayered coatings were prepared by changing the bias voltage during the deposition. LCI and LCII values were not improved by increasing the number of layers. The critical loads of the single-layered coatings decreased with increasing the bias voltage. It appears that, for the multilayered coatings, the combination of bias voltages influenced the critical loads. The critical loads strongly depended on dynamic hardness and Young’s modulus. In particular, the critical loads of the multilayered coatings were influenced by the properties of the intermediate and bottom layers as well as the surface roughness, hardness and Young’s modulus of the top layer. The large film delamination for single-layered coatings deposited using a high bias voltage occurred during pin-on-disk wear tests even though the critical loads of the single-layered coatings were higher than those of the multilayered coatings. If the brittle top layer could be broken and delaminated by the sliding contact, the ductile bottom layer coated under a bias voltage of 0V could endure the complete delamination of film.
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