Sr2(P2O7):Tb3+, Ce3+的制备及其发光性能

You-Dong Li, Limin Dong, Zongyuan Li, Lin Sun, Xianyou Zhang
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引用次数: 0

摘要

采用化学共沉淀法成功制备了Sr2(P2O7):Ce3+, Tb3+发光材料。采用扫描电子显微镜(SEM)、x射线衍射仪(XRD)和光致发光仪(PL)研究了材料的相结构、表面形貌和荧光性质。结果表明,该发光材料由纯Sr2(P2O7)相组成,没有出现稀土磷酸盐相。SEM显微图显示,在1100℃下合成的发光材料颗粒均匀,结晶度好。荧光光谱显示,当nSr: nTb= 100: 1, nTb: nCe=2:3,烧结温度为1100℃,保温时间为3h时,发光材料的荧光效果最好。
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Preparation and luminescent properties of Sr2(P2O7):Tb3+, Ce3+
We have successfully prepared the luminescent material of Sr2(P2O7):Ce3+, Tb3+ by the method of the chemical co-precipitation. The phase structure, surface morphology and fluorescence properties were investigated by the scanning electronic microscopy (SEM), X-ray diffraction (XRD), and photoluminescence (PL). It showed that the luminescent material is composed of the pure Sr2(P2O7) phase, and there no phases of rare earth phosphate appeared. The SEM micrographs showed uniform particles with good crystallinity of luminescent material synthesized at 1100°C. PL spectrum showed the luminescent material fluorescence effect best with nSr: nTb= 100: 1, nTb: nCe=2:3, sintering at 1100°C, the optimal heat preservation time was 3h.
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