M. R. Herrera-Rivera, Ana M. Pineda, A. Maldonado-Alvarez, M. D. L. L. Olvera-Amador
{"title":"均相沉淀法制备不同ZnO结构","authors":"M. R. Herrera-Rivera, Ana M. Pineda, A. Maldonado-Alvarez, M. D. L. L. Olvera-Amador","doi":"10.1109/ICEEE.2015.7357957","DOIUrl":null,"url":null,"abstract":"Mesoporous structures of zinc oxide (ZnO) powders were prepared by the homogenous precipitation method. ZnO nanoparticles were synthesized from a solution of zinc acetate dihydrate (Zn(CH3COO)2.2H2O) as zinc source and ammonium carbonate ((NH4)2CO3) as precipitant agent. Structural and morphological characteristics were studied with respect to changes in molarity (0.05, 0.5, and 0.35 M), percentage of saturation, synthesis temperature (30, and 70°C), and time (30, 60, and 120 min). ZnO phases were confirmed from X-ray Diffraction (XRD) results. The particles morphology (size and shape) was analyzed from the Transmission Electron Microscopy (TEM) and Scanning Electron Microscopy (SEM) characterization.","PeriodicalId":285783,"journal":{"name":"2015 12th International Conference on Electrical Engineering, Computing Science and Automatic Control (CCE)","volume":"24 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2015-12-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Different ZnO structures prepared by homogeneous precipitation method\",\"authors\":\"M. R. Herrera-Rivera, Ana M. Pineda, A. Maldonado-Alvarez, M. D. L. L. Olvera-Amador\",\"doi\":\"10.1109/ICEEE.2015.7357957\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Mesoporous structures of zinc oxide (ZnO) powders were prepared by the homogenous precipitation method. ZnO nanoparticles were synthesized from a solution of zinc acetate dihydrate (Zn(CH3COO)2.2H2O) as zinc source and ammonium carbonate ((NH4)2CO3) as precipitant agent. Structural and morphological characteristics were studied with respect to changes in molarity (0.05, 0.5, and 0.35 M), percentage of saturation, synthesis temperature (30, and 70°C), and time (30, 60, and 120 min). ZnO phases were confirmed from X-ray Diffraction (XRD) results. The particles morphology (size and shape) was analyzed from the Transmission Electron Microscopy (TEM) and Scanning Electron Microscopy (SEM) characterization.\",\"PeriodicalId\":285783,\"journal\":{\"name\":\"2015 12th International Conference on Electrical Engineering, Computing Science and Automatic Control (CCE)\",\"volume\":\"24 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2015-12-17\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"2015 12th International Conference on Electrical Engineering, Computing Science and Automatic Control (CCE)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/ICEEE.2015.7357957\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"2015 12th International Conference on Electrical Engineering, Computing Science and Automatic Control (CCE)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/ICEEE.2015.7357957","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Different ZnO structures prepared by homogeneous precipitation method
Mesoporous structures of zinc oxide (ZnO) powders were prepared by the homogenous precipitation method. ZnO nanoparticles were synthesized from a solution of zinc acetate dihydrate (Zn(CH3COO)2.2H2O) as zinc source and ammonium carbonate ((NH4)2CO3) as precipitant agent. Structural and morphological characteristics were studied with respect to changes in molarity (0.05, 0.5, and 0.35 M), percentage of saturation, synthesis temperature (30, and 70°C), and time (30, 60, and 120 min). ZnO phases were confirmed from X-ray Diffraction (XRD) results. The particles morphology (size and shape) was analyzed from the Transmission Electron Microscopy (TEM) and Scanning Electron Microscopy (SEM) characterization.