向日葵油与己二酸在不同温度下的聚合反应

Safa fakhri Kadouri, Ghalib Adrees Atiya Ali, Abdul Muniem Abbas Karim
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摘要

所制备的聚合物包括:聚(甘油三酯- alt -己二酸酯),表示它,已分为两步制备:第一步:在催化剂(pbO2)存在下,将甘油与葵花籽油反应(甘油三酯反应)在150℃下,使用电动搅拌器搅拌5小时,制备单体。第二步:这一步包括聚合过程(冷凝),以制备(醇酯树脂),其中单体(单甘油酯)是通过与(己二酸)在不同的温度下(150至240)反应而制备的,每次反应之间相差10℃,使用电子温度计控制温度,并使用磁铁棒在氮气(惰性气氛)存在下连续搅拌。计算了反应动力学,包括两个过程。第一个过程,即反应动力学,是通过跟踪聚合过程中酸值浓度的下降来实现的。关键词:葵花籽油,己二酸,PbO2催化剂
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Polymerization of sunflower oil with adipic acid using Catalyst at different temperatures
The polymers that have been prepared include the following: Poly(glyceride-ALT-adipate), which symbolizes it, has been prepared in two steps: The first step: Prepare the monomer from the reaction of glycerin with sunflower oil (glyceride reaction) in the presence of catalysts (pbO2) at a temperature of 150 and using the Electrical Stirrer for 5 hours. The second step: This step includes the polymerization process (condensation) in order to prepare (Alkyd Resin), where the monomer (Monoglyceride) is prepared by reacting with (Adipic acid) at different temperatures starting from (150 to 240 with a difference of 10 ℃ between one reaction and another using an electronic thermometer to control the temperature and with continuous stirring using a magnet bar and in the presence of nitrogen gas (inert atmosphere). The reaction kinetics is also calculated, which includes two processes. The first process, the kinetics of the reaction, is made by tracking the decrease in the concentration of acid value, which is made by the polymerization process. Keywords: sunflower oil, adipic acid, PbO2 Catalyst.
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