基于溶液的脉冲激光沉积法合成多金属纳米颗粒

A. Sellinger, T. Aburada, J. Fitz-Gerald
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引用次数: 8

摘要

采用激光辅助干法合成了多组分贵金属纳米颗粒。结合传统脉冲激光沉积和基质辅助脉冲激光蒸发的特性,在金属前驱体的Si衬底和电子显微镜网格上沉积了Au-Ag和Au-Ag- pd纳米颗粒。Au-Ag粒子的平均直径约为2.8 nm, Au-Ag- pd粒子的平均直径约为2.2 nm。在沉积颗粒中观察到显著的成分不均匀性,这归因于目标溶液的不均匀性和所选材料系统的分解行为。
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Synthesis of multimetallic nanoparticles using a solution-based pulsed laser deposition approach
Multicomponent noble metal nanoparticles were synthesized using a novel laser-assisted dry processing approach. Combining attributes from conventional pulsed laser deposition and matrix-assisted pulsed laser evaporation, nanoparticles of Au-Ag and Au-Ag-Pd were deposited on Si substrates and electron microscopy grids from metal precursors. The mean diameter of Au-Ag particles was approximately 2.8 nm, while that of Au-Ag-Pd particles was approximately 2.2 nm. Significant compositional non-uniformity was observed in deposited particles and is attributed to the inhomogeneity of the target solutions and the decomposition behavior of the selected material systems.
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