l -精氨酸稳定金纳米粒子表面等离子体共振的研究

Amaria Amaria, D. K. Maharani, M. M. Sianita
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引用次数: 0

摘要

-合成了l -精氨酸包封的金纳米颗粒(AuNP)。在本文中,我们报告了观察六周的纳米颗粒的稳定性。在本研究中,以柠檬酸三钠和旋盖剂l -精氨酸为稳定剂,将Au(III)还原为Au(0)合成了金纳米颗粒。本研究的参数为培养基的pH(5和10)和精氨酸的浓度(1、2和5 mM)。利用紫外-可见分光光度计测量表面等离子体共振光谱,从全宽半最大吸收的最大波长强度位置研究了金纳米粒子的稳定性。结果表明,通过红宝石溶液的出现,成功地合成了金纳米颗粒。pH值为10时表面等离子体共振谱比pH值为5时更清晰。在pH值为10的条件下,l -精氨酸可以在1-2.5 mM的浓度下稳定金纳米颗粒(AuNP)。通过研究表面共振等离子体光谱的λ max、峰强度和全宽半最大值的位置变化,证明了AuNP稳定的氨基酸l-精氨酸持续了6周。这些结果证明,AuNP-arg可以用于商业应用,如传感器或医疗和化妆品领域。
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Study of Surface Plasmon Resonance of Gold Nanoparticles Stabilized by L-arginine
- Gold nanoparticles (AuNP) capped by L-arginine have been synthesized. In this paper, we report the stability of nanoparticles observed for six weeks. In this study, gold nanoparticles were synthesized by reducing Au(III) to Au(0) using trisodium citrate and capping agent L-arginine as a stabilizer. The parameters of this study are the pH of the medium (5 and 10) and the concentration of-arginine (1, 2, and 5 mM). The stability of gold nanoparticles was studied from the position of the maximum wavelength intensity of the full-width half-maximum absorption from the surface plasmon resonance spectra measured by UV-vis spectrophotometer. The results showed that gold nanoparticles were successfully synthesized by the appearance of a ruby red solution. The spectra of surface plasmon resonance AuNP-arg pH 10 shows sharper than pH 5. Gold nanoparticles (AuNP) can be stabilized using L-arginine at concentrations of 1-2.5 mM under pH 10. AuNP stabilized amino acid L-arginine was shown for a period of six weeks through the study of position changes of λ max , peak intensity and a full-width half-maximum of surface resonance plasmon spectra. These results prove that AuNP-arg can be used in commercial applications, as sensors or in the medical and cosmetic fields.
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