壳聚糖纳米颗粒增强淀粉- g -聚4-丙烯酰胺苯甲酸的抗菌活性和溶胀能力

IF 1.3 4区 农林科学 Q2 MATERIALS SCIENCE, PAPER & WOOD Cellulose Chemistry and Technology Pub Date : 2023-09-29 DOI:10.35812/cellulosechemtechnol.2023.57.71
NAHED A. ABD EL-GHANY, MOHAMED S. ABDEL AZIZ, MARWA M. ABDEL-AZIZ, ZAIN M. MAHMOUD
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引用次数: 0

摘要

将淀粉接枝的聚丙烯酰胺苯甲酸(St-g-P4ABA)与壳聚糖纳米颗粒(csnp)(根据接枝质量分别为1%和3%)结合,制备了St-g-P4ABA/CSNPs1%和St-g-P4ABA/CSNPs3%纳米复合材料。采用核磁共振(1H NMR)、傅里叶变换红外光谱(FTIR)、扫描电镜(SEM)、透射电镜(TEM)和x射线衍射等手段对纳米复合材料的成功合成进行了验证。csnp的加入显著提高了St-g-P4ABA共聚物在水和0.9%盐水溶液中的热稳定性和溶胀度,尤其是在盐水溶液中。与St-g-P4ABA相比,St-g-P4ABA/CSNP复合物对革兰氏阳性菌、革兰氏阴性菌和真菌具有更好的抗菌活性。
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REINFORCEMENT OF ANTIMICROBIAL ACTIVITY AND SWELLING ABILITY OF STARCH-G-POLY 4-ACRYLAMIDOBENZOIC ACID USING CHITOSAN NANOPARTICLES
New nanocomposites, denoted as St-g-P4ABA/CSNPs1% and St-g-P4ABA/CSNPs3%, were created by combining starch-grafted polyacrylamide benzoic acid (St-g-P4ABA) with chitosan nanoparticles (CSNPs) (1% and 3% based on graft weight). Nuclear magnetic resonance (1H NMR), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray diffraction were used to clarify the successful synthesis of the nanocomposite. The thermal stability of St-g-P4ABA copolymer and its degree of swellability in both water and 0.9% saline solutions significantly improved as a result of the incorporation of CSNPs, most notably in the saline solution. When compared to St-g-P4ABA, the St-g-P4ABA/CSNP composites showed better antibacterial activity against Gram-positive bacteria, Gram-negative bacteria and fungi.
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来源期刊
Cellulose Chemistry and Technology
Cellulose Chemistry and Technology 工程技术-材料科学:纸与木材
CiteScore
2.30
自引率
23.10%
发文量
81
审稿时长
7.3 months
期刊介绍: Cellulose Chemistry and Technology covers the study and exploitation of the industrial applications of carbohydrate polymers in areas such as food, textiles, paper, wood, adhesives, pharmaceuticals, oil field applications and industrial chemistry. Topics include: • studies of structure and properties • biological and industrial development • analytical methods • chemical and microbiological modifications • interactions with other materials
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