{"title":"探索烟酸铀酰的性质:合成、表征和热分析","authors":"Assis de, Carvalho de, Colman Denck","doi":"10.2298/jsc230817071a","DOIUrl":null,"url":null,"abstract":"This study reports the successful synthesis and characterization of a uranyl nicotinate compound, UO2(C6H4NO2)2?0.25H2O. The compound was synthesized using a Metal 1:2 Ligand ratio and water as the solvent. The average yield of the compound was found to be 67%. Thermogravimetric analysis revealed multiple stages of mass loss, including dehydration, nitrogen decomposition, and UO22+ reduction. Fourier-transform infrared spectroscopy confirmed the coordination of the carboxylate group in the compound. Field emission gun scanning electron microscope analysis showed particles with a regular oval shape. Energy-dispersive X-ray spectroscopy provided semi-quantitative data on the elemental composition of the compound. The major elements identified were uranium, carbon, oxygen, and nitrogen. These results contribute to understanding the compound's synthesis, thermal behavior, molecular composition, particle morphology, and elemental composition. Further research can build upon these findings to explore potential applications and develop new compounds with tailored properties","PeriodicalId":17489,"journal":{"name":"Journal of The Serbian Chemical Society","volume":null,"pages":null},"PeriodicalIF":1.0000,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Exploring the properties of uranyl nicotinate: Synthesis, characterization, and thermal analysis\",\"authors\":\"Assis de, Carvalho de, Colman Denck\",\"doi\":\"10.2298/jsc230817071a\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"This study reports the successful synthesis and characterization of a uranyl nicotinate compound, UO2(C6H4NO2)2?0.25H2O. The compound was synthesized using a Metal 1:2 Ligand ratio and water as the solvent. The average yield of the compound was found to be 67%. Thermogravimetric analysis revealed multiple stages of mass loss, including dehydration, nitrogen decomposition, and UO22+ reduction. Fourier-transform infrared spectroscopy confirmed the coordination of the carboxylate group in the compound. Field emission gun scanning electron microscope analysis showed particles with a regular oval shape. Energy-dispersive X-ray spectroscopy provided semi-quantitative data on the elemental composition of the compound. The major elements identified were uranium, carbon, oxygen, and nitrogen. These results contribute to understanding the compound's synthesis, thermal behavior, molecular composition, particle morphology, and elemental composition. Further research can build upon these findings to explore potential applications and develop new compounds with tailored properties\",\"PeriodicalId\":17489,\"journal\":{\"name\":\"Journal of The Serbian Chemical Society\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":1.0000,\"publicationDate\":\"2023-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of The Serbian Chemical Society\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2298/jsc230817071a\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of The Serbian Chemical Society","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2298/jsc230817071a","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}
Exploring the properties of uranyl nicotinate: Synthesis, characterization, and thermal analysis
This study reports the successful synthesis and characterization of a uranyl nicotinate compound, UO2(C6H4NO2)2?0.25H2O. The compound was synthesized using a Metal 1:2 Ligand ratio and water as the solvent. The average yield of the compound was found to be 67%. Thermogravimetric analysis revealed multiple stages of mass loss, including dehydration, nitrogen decomposition, and UO22+ reduction. Fourier-transform infrared spectroscopy confirmed the coordination of the carboxylate group in the compound. Field emission gun scanning electron microscope analysis showed particles with a regular oval shape. Energy-dispersive X-ray spectroscopy provided semi-quantitative data on the elemental composition of the compound. The major elements identified were uranium, carbon, oxygen, and nitrogen. These results contribute to understanding the compound's synthesis, thermal behavior, molecular composition, particle morphology, and elemental composition. Further research can build upon these findings to explore potential applications and develop new compounds with tailored properties
期刊介绍：
The Journal of the Serbian Chemical Society -JSCS (formerly Glasnik Hemijskog društva Beograd) publishes articles original papers that have not been published previously, from the fields of fundamental and applied chemistry:
Theoretical Chemistry, Organic Chemistry, Biochemistry and Biotechnology, Food Chemistry, Technology and Engineering, Inorganic Chemistry, Polymers, Analytical Chemistry, Physical Chemistry, Spectroscopy, Electrochemistry, Thermodynamics, Chemical Engineering, Textile Engineering, Materials, Ceramics, Metallurgy, Geochemistry, Environmental Chemistry, History of and Education in Chemistry.
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