小角度几何电子衍射图中菊池线的识别。

IF 1.9 4区 材料科学 Q3 CHEMISTRY, MULTIDISCIPLINARY Acta Crystallographica Section A: Foundations and Advances Pub Date : 2024-01-01 DOI:10.1107/S2053273323009385
Zbigniew Mitura, Grzegorz Szwachta, Łukasz Kokosza, Marek Przybylski
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引用次数: 0

摘要

结果表明,如果使用数字图像处理软件对反射高能电子衍射(RHEED)模式进行滤波,则菊池特征变得清晰可见。对于在入射电子束不同方位角处收集的数据,显示了具有混合表面终止的SrTiO3的这种模式转换的结果。提出并讨论了过滤后菊池图案理论描述的一种简化解析方法。给出了薄膜的原始图样和过滤图样的一些例子。RHEED模式可以看作是电子波相干和非相干散射的结果。相干散射的影响可以被认为是由理想晶体的波衍射引起的,通常,只有分析这种类型的影响才能获得使用RHEED研究的样品的结构信息。然而,一些主要由原子的热振动引起的非相干散射效应,称为菊池效应,也可能是关于表面附近原子排列的有价值信息的来源。通常,对于RHEED,菊池特征隐藏在强度背景中,研究人员不容易识别。本文表明,使用计算机图形学方法可以大大增强这类特征的可见性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Identification of Kikuchi lines in electron diffraction patterns collected in small-angle geometry.

It is demonstrated that Kikuchi features become clearly visible if reflection high-energy electron diffraction (RHEED) patterns are filtered using digital image processing software. The results of such pattern transformations are shown for SrTiO3 with mixed surface termination for data collected at different azimuths of the incident electron beam. A simplified analytical approach for the theoretical description of filtered Kikuchi patterns is proposed and discussed. Some examples of raw and filtered patterns for thin films are shown. RHEED patterns may be treated as a result of coherent and incoherent scattering of electron waves. The effects of coherent scattering may be considered as those occurring due to wave diffraction by an idealized crystal and, usually, only effects of this type are analysed to obtain structural information on samples investigated with the use of RHEED. However, some incoherent scattering effects mostly caused by thermal vibrations of atoms, known as Kikuchi effects, may also be a source of valuable information on the arrangements of atoms near the surface. Typically, for the case of RHEED, Kikuchi features are hidden in the intensity background and researchers cannot easily recognize them. In this paper, it is shown that the visibility of features of this type can be substantially enhanced using computer graphics methods.

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来源期刊
Acta Crystallographica Section A: Foundations and Advances
Acta Crystallographica Section A: Foundations and Advances CHEMISTRY, MULTIDISCIPLINARYCRYSTALLOGRAPH-CRYSTALLOGRAPHY
CiteScore
2.60
自引率
11.10%
发文量
419
期刊介绍: Acta Crystallographica Section A: Foundations and Advances publishes articles reporting advances in the theory and practice of all areas of crystallography in the broadest sense. As well as traditional crystallography, this includes nanocrystals, metacrystals, amorphous materials, quasicrystals, synchrotron and XFEL studies, coherent scattering, diffraction imaging, time-resolved studies and the structure of strain and defects in materials. The journal has two parts, a rapid-publication Advances section and the traditional Foundations section. Articles for the Advances section are of particularly high value and impact. They receive expedited treatment and may be highlighted by an accompanying scientific commentary article and a press release. Further details are given in the November 2013 Editorial. The central themes of the journal are, on the one hand, experimental and theoretical studies of the properties and arrangements of atoms, ions and molecules in condensed matter, periodic, quasiperiodic or amorphous, ideal or real, and, on the other, the theoretical and experimental aspects of the various methods to determine these properties and arrangements.
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