通过真空烧结工艺在 Ti-8Nb-4Co 合金中添加 Mo2C 粉末对微观结构和强化机制的影响

IF 0.7 4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Archives of Metallurgy and Materials Pub Date : 2023-12-19 DOI:10.24425/amm.2023.146190
Shih-Hsien Chang, Kun-Jie Liao, K. Huang, Cheng Liang
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引用次数: 0

摘要

本研究利用粉末冶金的真空烧结工艺,在 Ti-8nb-4Co 合金中加入不同比例的 Mo 2 C 粉末(1、3 和 5 质量%),同时分别在 1240、1270、1300 和 1330°C 下真空烧结合金 1 小时。实验结果表明,当在 Ti-8nb-4Co 合金中添加 3 质量%的 Mo 2 C 粉末时,试样在 1300°C 下烧结 1 小时后具有最佳的机械性能,相对密度为 98.此外,真空烧结 Ti-8nb-4Co-3Mo 2 C 合金的微观结构具有 α 和 β 相结构以及 TiC 沉淀。EBSD 结果证实,Mo 2 C 在烧结过程中原位生成了 TiC,并均匀地分散在晶界中。此外,还原钼原子在钛基体中起到了β相稳定元素和固溶体的作用。
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Effects of the Microstructure and Strengthening Mechanisms of Mo2C Powders Being Added to Ti-8Nb-4Co Alloy Via the Vacuum Sintering Process
This study utilizes Ti-8nb-4Co alloys added to different proportions of Mo 2 C powders (1, 3, and 5 mass%) by the vacuum sintering process of powder metallurgy and simultaneously vacuum sinters the alloys at 1240, 1270, 1300, and 1330°C for 1 h, respectively. The experimental results indicate that when 3 mass% Mo 2 C powders were added to the Ti-8nb-4Co alloys, the specimens possessed the optimal mechanical properties after sintering at 1300°C for 1 h. The relative density was 98.02%, and the hardness and TRS were enhanced to 69.6 hRa and 1816.7 MPa, respectively. in addition, the microstructure of vacuum sintered Ti-8nb-4Co-3Mo 2 C alloys has both α and β-phase structures, as well as TiC precipitates. EBSD results confirm that the Mo 2 C in situ produced TiC during the sintering process and was uniformly dispersed in the grain boundary. Moreover, the reduced molybdenum atom acted as a β-phase stabilizing element and solid-solution in the titanium matrix.
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来源期刊
Archives of Metallurgy and Materials
Archives of Metallurgy and Materials 工程技术-冶金工程
CiteScore
1.20
自引率
0.00%
发文量
0
审稿时长
4.5 months
期刊介绍: The Archives of Metallurgy and Materials is covered in the following Institute for Scientific Information products: SciSearch (the Science Citation Index - Expanded), Research Alert, Materials Science Citation Index, and Current Contents / Engineering, Computing and Technology. Articles published in the Archives of Metallurgy and Materials are also indexed or abstracted by Cambridge Scientific Abstracts.
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