用原子分辨电子显微镜检测晶体中原子的小位移。

H Hashimoto, M Kuwabara, Y Takai, S Tsubokawa, Y Yokota
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引用次数: 4

摘要

介绍了晶体中原子位移检测的四种工作。在Au晶体的电子显微镜图像中发现了不规则的小原子位移,其精度约为0.1 A。原子像的位移由无像差聚焦(AFF)记录。即使当SiC和TaS2晶体中原子的周期性位移约为晶格常数的0.1%时,这种位移也会在图像中显示为弱对比异常。利用附在电子显微镜上的电视系统进行现场观察,记录下了在1/30秒内发生的原子的快速运动。利用电视系统图像连续相减和图像sigma技术,每1/10秒只记录金晶体中运动原子的图像。
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Detection of small displacement of atoms in crystals by atom resolution electron microscopy.

Four kinds of works on the detection of displacement of atoms in crystals are shown. The irregular small displacement of atoms has been detected, with an accuracy of about 0.1 A around dislocations and stacking faults in Au crystals as shown by their electron microscope images. The displacement of the atomic images is recorded by aberration-free focus (AFF). Even when the periodic displacement of atoms in SiC and TaS2 crystals is around 0.1% of the lattice constant, this displacement has been revealed as the weak-contrast anomaly in the images. Using in situ observations by a TV system attached to an electron microscope, the rapid movements of atoms that have taken place within 1/30 sec have been recorded. Using the technique of successive subtraction of the images by TV system and image sigma, only the images of moving atoms in Au crystal have been recorded each 1/10 sec.

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