微波辅助一步法生物合成二氧化钛纳米颗粒:抗菌、抗氧化和光催化特性

IF 1.2 4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Kuwait Journal of Science Pub Date : 2024-02-08 DOI:10.1016/j.kjs.2024.100203
Waseem Ahmad , Sanjay Kumar , Sarfaraz Ahmed
{"title":"微波辅助一步法生物合成二氧化钛纳米颗粒:抗菌、抗氧化和光催化特性","authors":"Waseem Ahmad ,&nbsp;Sanjay Kumar ,&nbsp;Sarfaraz Ahmed","doi":"10.1016/j.kjs.2024.100203","DOIUrl":null,"url":null,"abstract":"<div><p>The present study provides an environmentally benevolent synthesis of titanium dioxide nanoparticles (TiO2 NPs). Morphological characteristics of the fabricated nanoparticles were assessed by using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and UV-Spectroscopy. The XRD pattern of the synthesized nanoparticles showed that the nanoparticles had a tetragonal crystalline structure with a particle size of 20–40 nm. The photocatalytic efficacy of the developed nanomaterials was investigated in relation to indigo carmine, bromothymol blue, and rhodamine b dye. The presence of a photocatalyst leads to an improved performance, causing a decline in dye concentration with increasing irradiation time. The highest dye degradation of about 95 % was observed against indigo carmine dye. The green synthesized TiO<sub>2</sub> NPs exhibited a significant zone of inhibition (23 mm) in antibacterial activity against <em>Bacillus</em> at the concentration of 70 mg/mL. The developed nanoparticles demonstrate 81.29 % DPPH radical scavenging activity at the concentration of 60 μg/mL.</p></div>","PeriodicalId":17848,"journal":{"name":"Kuwait Journal of Science","volume":null,"pages":null},"PeriodicalIF":1.2000,"publicationDate":"2024-02-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S2307410824000282/pdfft?md5=fc316a1772e7d33c362993ef7ef98273&pid=1-s2.0-S2307410824000282-main.pdf","citationCount":"0","resultStr":"{\"title\":\"Microwave-assisted one-step biosynthesis of titanium dioxide nanoparticles: Antibacterial, antioxidant, and photocatalytic properties\",\"authors\":\"Waseem Ahmad ,&nbsp;Sanjay Kumar ,&nbsp;Sarfaraz Ahmed\",\"doi\":\"10.1016/j.kjs.2024.100203\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>The present study provides an environmentally benevolent synthesis of titanium dioxide nanoparticles (TiO2 NPs). Morphological characteristics of the fabricated nanoparticles were assessed by using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and UV-Spectroscopy. The XRD pattern of the synthesized nanoparticles showed that the nanoparticles had a tetragonal crystalline structure with a particle size of 20–40 nm. The photocatalytic efficacy of the developed nanomaterials was investigated in relation to indigo carmine, bromothymol blue, and rhodamine b dye. The presence of a photocatalyst leads to an improved performance, causing a decline in dye concentration with increasing irradiation time. The highest dye degradation of about 95 % was observed against indigo carmine dye. The green synthesized TiO<sub>2</sub> NPs exhibited a significant zone of inhibition (23 mm) in antibacterial activity against <em>Bacillus</em> at the concentration of 70 mg/mL. The developed nanoparticles demonstrate 81.29 % DPPH radical scavenging activity at the concentration of 60 μg/mL.</p></div>\",\"PeriodicalId\":17848,\"journal\":{\"name\":\"Kuwait Journal of Science\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":1.2000,\"publicationDate\":\"2024-02-08\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.sciencedirect.com/science/article/pii/S2307410824000282/pdfft?md5=fc316a1772e7d33c362993ef7ef98273&pid=1-s2.0-S2307410824000282-main.pdf\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Kuwait Journal of Science\",\"FirstCategoryId\":\"103\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S2307410824000282\",\"RegionNum\":4,\"RegionCategory\":\"综合性期刊\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"MULTIDISCIPLINARY SCIENCES\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Kuwait Journal of Science","FirstCategoryId":"103","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2307410824000282","RegionNum":4,"RegionCategory":"综合性期刊","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MULTIDISCIPLINARY SCIENCES","Score":null,"Total":0}
引用次数: 0

摘要

本研究提供了一种对环境无害的二氧化钛纳米粒子(TiO2 NPs)合成方法。利用 X 射线衍射(XRD)、傅立叶变换红外光谱(FTIR)、扫描电子显微镜(SEM)和紫外光谱评估了所制备纳米粒子的形态特征。合成纳米粒子的 XRD 图谱显示,纳米粒子具有四方晶体结构,粒径为 20-40 纳米。研究了所开发的纳米材料对靛胭脂红、溴百里酚蓝和罗丹明 b 染料的光催化功效。光催化剂的存在提高了性能,使染料浓度随着照射时间的延长而下降。对靛胭脂红染料的降解率最高,约为 95%。在 70 毫克/毫升的浓度下,绿色合成的 TiO2 NPs 对芽孢杆菌具有显著的抑菌作用(23 毫米)。在浓度为 60 μg/mL 时,所开发的纳米粒子显示出 81.29 % 的 DPPH 自由基清除活性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Microwave-assisted one-step biosynthesis of titanium dioxide nanoparticles: Antibacterial, antioxidant, and photocatalytic properties

The present study provides an environmentally benevolent synthesis of titanium dioxide nanoparticles (TiO2 NPs). Morphological characteristics of the fabricated nanoparticles were assessed by using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and UV-Spectroscopy. The XRD pattern of the synthesized nanoparticles showed that the nanoparticles had a tetragonal crystalline structure with a particle size of 20–40 nm. The photocatalytic efficacy of the developed nanomaterials was investigated in relation to indigo carmine, bromothymol blue, and rhodamine b dye. The presence of a photocatalyst leads to an improved performance, causing a decline in dye concentration with increasing irradiation time. The highest dye degradation of about 95 % was observed against indigo carmine dye. The green synthesized TiO2 NPs exhibited a significant zone of inhibition (23 mm) in antibacterial activity against Bacillus at the concentration of 70 mg/mL. The developed nanoparticles demonstrate 81.29 % DPPH radical scavenging activity at the concentration of 60 μg/mL.

求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Kuwait Journal of Science
Kuwait Journal of Science MULTIDISCIPLINARY SCIENCES-
CiteScore
1.60
自引率
28.60%
发文量
132
期刊介绍: Kuwait Journal of Science (KJS) is indexed and abstracted by major publishing houses such as Chemical Abstract, Science Citation Index, Current contents, Mathematics Abstract, Micribiological Abstracts etc. KJS publishes peer-review articles in various fields of Science including Mathematics, Computer Science, Physics, Statistics, Biology, Chemistry and Earth & Environmental Sciences. In addition, it also aims to bring the results of scientific research carried out under a variety of intellectual traditions and organizations to the attention of specialized scholarly readership. As such, the publisher expects the submission of original manuscripts which contain analysis and solutions about important theoretical, empirical and normative issues.
期刊最新文献
Editorial Board Design, synthesis, and structural investigations of novel (S)-amide derivatives as promising ACE inhibitors Mixture design as an innovative tool to optimize the antioxidant and antibacterial activity of moroccan essential oils: Clinopodium nepeta, Ruta montana, and Dittrichia viscosa Optimization of microwave-assisted extraction to obtain a polyphenol-rich crude extract from duku (Lansium domesticum Corr.) leaf and the correlation with antioxidant and cytotoxic activities The use of mint and thyme extracts as eco–friendly natural dyes and the antimicrobial properties of dyed products
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1