超声波辅助下的酸橙皮真空干燥及其热、形态和功能特性表征

IF 5.1 3区 工程技术 Q2 ENERGY & FUELS Thermal Science and Engineering Progress Pub Date : 2024-09-01 DOI:10.1016/j.tsep.2024.102841
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引用次数: 0

摘要

这项研究旨在确定使用超声波辅助真空干燥(UAVD)、真空辅助干燥(VAD)、烘箱干燥(OD)和真空干燥(VD)干燥的酸橙皮的干燥行为和能耗,并通过能效分析(包括特定水分提取率(SMER)、水分提取率(MER)和特定能耗(SEC))研究干燥果皮的热重分解、形态、元素和光谱分析。与 OD、VAD 和 VD 相比,UAVD 的干燥时间分别缩短了 49%、34% 和 15%。UAVD 的干燥速率最高。有效水分扩散率(Deff)值从高到低依次为 UAVD>VD>VAD>OD。近似物分析表明,使用 UAVD 干燥的酸橙皮的固定碳(25.35 %)和灰分(3.03 %)含量最高,但挥发物(61.68 %)含量最低。干燥的石灰桔皮表现出相似的热分解行为。UAVD 造成了多孔和粗糙表面的形成以及微通道效应。碳(62.56%)和氧(15.98%)是干酸橙皮中的主要元素。使用 UAVD 干燥的酸橙皮的 O/C 比(0.25)和 H/C 比(0.85)最低。傅立叶变换红外光谱(FTIR)主要显示 O-H、C-H、CO、CC 和 C-O-C 伸展振动。UAVD 的 SMER(0.0053 千克/千瓦时)和 MER(0.0012 千克/小时)值最高,SEC(188.27 千瓦时/千克)值最低。总之,UAVD 是干燥酸橙皮最合适的干燥方法。
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Ultrasound-assisted vacuum drying of limequat peels and characterization of thermal, morphological and functional properties

This work aimed to determine drying behavior and energy consumption of limequat peels dried using ultrasound-assisted vacuum drying (UAVD), vacuum-assisted drying (VAD), oven drying (OD) and vacuum drying (VD), and investigate thermogravimetric decomposition, morphological, elemental and spectral analyses of dried peels with energy efficiency analysis including specific moisture extraction rate (SMER), moisture extraction rate (MER) and specific energy consumption (SEC). The UAVD considerably shortened drying time by 49 %, 34 % and 15 % as compared to the OD, VAD and VD. The highest drying rate was achieved at the UAVD. The effective moisture diffusivity (Deff) values in descending order were UAVD>VD>VAD>OD. Proximate analysis showed that limequat peels dried using the UAVD had the highest fixed carbon (25.35 %) and ash (3.03 %) contents, but the lowest volatile matter (61.68 %). Dried limequat peels exhibited similar thermal decomposition behavior. The UAVD caused porous and rough surface formation, and microchanneling effect. Carbon (>62.56 %) and oxygen (>15.98 %) were the major elements in dried limequat peels. The lowest O/C (0.25) and H/C (0.85) ratios were obtained for the limequat peels dried using the UAVD. Fourier-transform infrared spectroscopy (FTIR) spectra showed primarily O–H, C–H, CO, CC and C–O–C stretching vibrations. The highest SMER (0.0053 kg/kWh) and MER (0.0012 kg/h) values, and the lowest SEC (188.27 kWh/kg) value were determined for the UAVD. In conclusion, the UAVD was found to be the most appropriate drying method for the drying of limequat peels.

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来源期刊
Thermal Science and Engineering Progress
Thermal Science and Engineering Progress Chemical Engineering-Fluid Flow and Transfer Processes
CiteScore
7.20
自引率
10.40%
发文量
327
审稿时长
41 days
期刊介绍: Thermal Science and Engineering Progress (TSEP) publishes original, high-quality research articles that span activities ranging from fundamental scientific research and discussion of the more controversial thermodynamic theories, to developments in thermal engineering that are in many instances examples of the way scientists and engineers are addressing the challenges facing a growing population – smart cities and global warming – maximising thermodynamic efficiencies and minimising all heat losses. It is intended that these will be of current relevance and interest to industry, academia and other practitioners. It is evident that many specialised journals in thermal and, to some extent, in fluid disciplines tend to focus on topics that can be classified as fundamental in nature, or are ‘applied’ and near-market. Thermal Science and Engineering Progress will bridge the gap between these two areas, allowing authors to make an easy choice, should they or a journal editor feel that their papers are ‘out of scope’ when considering other journals. The range of topics covered by Thermal Science and Engineering Progress addresses the rapid rate of development being made in thermal transfer processes as they affect traditional fields, and important growth in the topical research areas of aerospace, thermal biological and medical systems, electronics and nano-technologies, renewable energy systems, food production (including agriculture), and the need to minimise man-made thermal impacts on climate change. Review articles on appropriate topics for TSEP are encouraged, although until TSEP is fully established, these will be limited in number. Before submitting such articles, please contact one of the Editors, or a member of the Editorial Advisory Board with an outline of your proposal and your expertise in the area of your review.
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