通过无压粘性烧结获得半透明持久发光玻璃基复合材料

IF 3 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Materialia Pub Date : 2024-09-05 DOI:10.1016/j.mtla.2024.102222
Roger Gomes Fernandes , Elaine de Andrade Mattos , Victor Murilo Poltronieri da Silva , David Van der Heggen , Philippe F. Smet , Danilo Manzani , Verônica de Carvalho Teixeira , Lucas Carvalho Veloso Rodrigues
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引用次数: 0

摘要

以硅酸盐玻璃为基体材料,采用无压粘性烧结法首次成功获得了半透明的持久发光玻璃基复合材料(PeL-GMCs)。首先,在还原气氛下通过微波辅助合成法制备了 SrAl2O4: Eu2+; Dy3+ 的持久发光微颗粒(PeL-MPs)。为了获得持久发光玻璃基复合材料,将 1 wt. % 的这些颗粒与钠钙硅酸盐玻璃珠混合并压制成颗粒。随后,通过无压粘性烧结对盘状样品进行热处理。尽管材料存在一些孔隙,但 PeL-GMCs 仍然表现出半透明性和长时间的持续发光(12 分钟)。此外,我们还注意到 PeL-MPs 与玻璃基体之间具有极佳的相容性,因为通过光学显微镜、能量色散 X 射线(EDX)图谱分析和扫描电镜阴极发光(CL)均未发现化学作用。此外,在制备材料后,颗粒的余辉强度保持不变。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Translucent persistent luminescence glass matrix composite obtained by pressureless viscous sintering

Translucent persistent luminescence glass matrix composites (PeL-GMCs) were successfully obtained for the first time using a pressureless viscous sintering method with silicate glass as the host material. Initially, persistent luminescence microparticles (PeL-MPs) of SrAl2O4: Eu2+; Dy3+ were prepared by microwave-assisted synthesis under a reducing atmosphere. To obtain persistent luminescent glass matrix composites, 1 wt. % of these particles were mixed with soda-lime-silicate glass beads and pressed into pellets. Subsequently, the disk-shaped samples were heat-treated through pressureless viscous sintering. Despite some material porosity, the PeL-GMCs exhibited translucency and prolonged persistent luminescence (12min). Additionally, we noted excellent compatibility between the PeL-MPs and the glass host, since no chemical interaction was found, as verified by optical microscopy, energy dispersive X-ray (EDX) mapping analysis and cathodoluminescence (CL) in SEM. Furthermore, the afterglow intensity of the particles was maintained after the preparation of materials.

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来源期刊
Materialia
Materialia MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
6.40
自引率
2.90%
发文量
345
审稿时长
36 days
期刊介绍: Materialia is a multidisciplinary journal of materials science and engineering that publishes original peer-reviewed research articles. Articles in Materialia advance the understanding of the relationship between processing, structure, property, and function of materials. Materialia publishes full-length research articles, review articles, and letters (short communications). In addition to receiving direct submissions, Materialia also accepts transfers from Acta Materialia, Inc. partner journals. Materialia offers authors the choice to publish on an open access model (with author fee), or on a subscription model (with no author fee).
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