打印室氧气含量对 3D 打印 316L 的微观结构和性能的影响

WY Wang, W Liu, A Godfrey
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摘要

利用激光粉末床熔融技术从同一批粉末中制备了 316L 不锈钢样品,并使用了不同的打印室氧含量(从 50 ppm 到 1500 ppm)。结果发现,氧化物颗粒密度随氧气含量的增加而增加,而晶胞结构则随氧气含量的变化而变化,当测量到的氧气含量超过 450 ppm 时,晶粒大小会出现相对急剧的变化。根据微观结构观察,氧含量的增加会导致凝固模式的转变。与氧含量较低、晶粒结构较粗的样品相比,氧含量较高的样品强度更高,机械各向异性更低。较高的氧化物颗粒含量对热稳定性的主要影响在于 1000 °C 等温退火过程中的再结晶动力学。
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Influence of print-chamber oxygen content on the microstructure and properties of 3D-printed 316L
Samples of 316L stainless steel have been prepared using laser-powder bed fusion from the same batch of powder using different print-chamber oxygen levels, ranging from 50 ppm to 1500 ppm. The oxide particle density is found to increase with oxygen content, while the cell structure is invariant with oxygen level and the grain size shows a relatively sharp transition for measured oxygen levels of above 450 ppm. Based on the microstructural observations it is suggested that the increasing oxygen levels leads to a transition in the solidification pattern. Samples printed at the higher oxygen level show higher strength and lower mechanical anisotropy than samples with a coarser grains structure printed at lower oxygen levels. The main influence of the higher oxide particle content on thermal stability is on the kinetics of recrystallization during isothermal annealing at 1000 °C.
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