通过火花等离子烧结 (SPS) 和真空热压 (VHP) 以及简单剪切挤压 (SSE) 生产的 Al/Al2O3 复合材料的机械性能和纹理发展得到增强

IF 6.2 2区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Materials Research and Technology-Jmr&t Pub Date : 2024-09-14 DOI:10.1016/j.jmrt.2024.09.079
Majed Zabihi, Esmaeil Emadoddin, Fathallah Qods
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引用次数: 0

摘要

通过粉末冶金法(PM)生产出了 Al-3vol% Al2O3 复合材料的绿色压实物,随后通过火花等离子烧结法(SPS)和真空热压法(VHP)对其进行了处理。然后用简单剪切挤压(SSE)工艺加工制成的样品。本研究使用了三种 SSE 模具,其变形角 (α)分别为 8°、10° 和 22.5°。α = 10° 的 SPS-ed/SSE-ed 试样成功变形达 16 次,而 VHP-ed/SSE-ed 试样则在 6 次变形后失效。此外,α = 22.5° 的 SPS-ed 样品只经历了一次 SSE。与真空烧结和搅拌铸造制造方法相比,SPS-ed/SSE-ed 复合材料的剪切冲压试验(SPT)载荷最高,孔隙率有所改善,增强材料的重新分布也最好,这一点已通过微观结构评估和孔隙率测量得到证实。在第 16 道工序中,使用 X 射线方法研究了 α = 10° 的 SPS-ed/SSE-ed 复合材料的结晶纹理。纹理发展结果表明,{100}<011>和{001}<100>组分的剪切纹理和立方体纹理强度非常低。
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Enhanced mechanical behavior and texture development of Al/Al2O3 composites produced by spark plasma sintering (SPS) and vacuum hot pressing (VHP) followed by simple shear extrusion (SSE)

Green compacts of Al-3vol% Al2O3 composites were produced by powder metallurgy (PM) and subsequently processed by spark plasma sintering (SPS) and vacuum hot pressing (VHP). The manufactured samples were then processed by the simple shear extrusion (SSE) process. Three SSE dies with the distortion angles (α) of 8°, 10° and 22.5° were used in this study. The SPS-ed/SSE-ed specimens for α = 10° were successfully deformed up to sixteen passes, while the VHP-ed/SSE-ed samples failed after six passes. In addition, the SPS-ed sample for α = 22.5° only underwent one pass of SSE. The SPS-ed/SSE-ed composites resulted in the highest shear punch test (SPT) load, modified porosity amount and the best reinforcement redistribution, as compared to the vacuum sintering and stir-casting manufacturing methods, which was confirmed by microstructure evaluation and porosity measurements. The crystallographic texture of the SPS-ed/SSE-ed composites for α = 10° was investigated in the sixteenth pass using the X-ray method. The results of texture development showed the very low intensity of shear and cube texture with {100} <011> and {001} <100> components, subsequently.

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来源期刊
Journal of Materials Research and Technology-Jmr&t
Journal of Materials Research and Technology-Jmr&t Materials Science-Metals and Alloys
CiteScore
8.80
自引率
9.40%
发文量
1877
审稿时长
35 days
期刊介绍: The Journal of Materials Research and Technology is a publication of ABM - Brazilian Metallurgical, Materials and Mining Association - and publishes four issues per year also with a free version online (www.jmrt.com.br). The journal provides an international medium for the publication of theoretical and experimental studies related to Metallurgy, Materials and Minerals research and technology. Appropriate submissions to the Journal of Materials Research and Technology should include scientific and/or engineering factors which affect processes and products in the Metallurgy, Materials and Mining areas.
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