通过低于 β 相变温度的背热辅助搅拌摩擦焊,实现中等厚度 Ti-6Al-4 V 合金接头的优异机械性能和腐蚀性能

IF 4.8 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2024-09-16 DOI:10.1016/j.matchar.2024.114391
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引用次数: 0

摘要

在钛合金的β相转变点以下形成的等轴微观结构通常在机械性能和耐腐蚀性能方面表现出极佳的平衡。然而,这种理想的微观结构不可能在熔融焊接接头中获得,但有望通过固态搅拌摩擦焊(FSW)技术实现。遗憾的是,在β相转变点以下进行传统的 FSW 时,中等厚度的钛合金接头通常会产生底部缺陷和严重的工具磨损。在这项研究中,6 毫米厚的 Ti-6Al-4 V 板通过传统的 FSW 和背加热辅助 FSW(BHAFSW)进行了连接。在传统的 FSW 过程中,出现了明显的工具磨损和底部相变差异造成的缺陷。研究发现,从 500 ℃ 到 900 ℃,母材 (BM) 和工具之间的硬度差增加到 35.6%。利用背温(150 °C)将焊接温度控制在 900 °C以下,从而通过增加硬度差在很大程度上减少了工具磨损。此外,背面温度补偿提高了底部温度,控制了相变位置从接头底部到中部的转变。肩部压力造成了缺陷的压缩,通过增加相变位置的压力,缺陷得以消除。通过背热辅助 FSW,在搅拌区的β相变温度以下形成了平均晶粒大小在 0.9 μm 以下的细化等轴晶微观结构,而在β相变温度附近形成了平均晶粒大小为 3.5 μm 的双峰结构。与 BM 相比,具有等轴晶微结构的接头(占 BM 的 98%)的强度明显降低,接头的耐腐蚀性能也有所增强。这种机械性能和耐腐蚀性能的卓越协同作用超过了之前报道的大多数钛合金接头。这项研究为获得具有超细等轴结构的中等厚度钛合金接头提供了一种有效的方法,这种接头具有优异的机械性能和耐腐蚀性能。
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Achieving superior mechanical and corrosion properties in medium-thickness Ti-6Al-4 V alloy joints by back heating assisted friction stir welding below β-phase transformation temperature
The equiaxed microstructure formed below the β-phase transition point of Ti alloys generally exhibits an excellent balance of mechanical properties and corrosion resistance. However, this desirable microstructure is impossible to be obtained in fusion welded joints but is prospective to be achieved by the solid-state friction stir welding (FSW) technique. Unfortunately, it generally generates bottom defects and severe tool wear in medium-thickness Ti alloy joints when conventional FSW was conducted below the β-phase transition point. In this study, 6 mm thick Ti-6Al-4 V plates were joined by both the conventional FSW and back heating assisted FSW (BHAFSW). Defects caused by significant tool wear and bottom phase transition differences occurred in the conventional FSW. It was found that the hardness difference between the base material (BM) and the tool increased to 35.6 % from 500 °C to 900 °C. The back heating (150 °C) was used to control welding temperatures remaining the 900 °C, thus largely reducing the tool wear by increasing the hardness difference. In addition, the back temperature compensation increased the bottom temperature and controlled the phase transition position from the bottom to the middle of the joint. The shoulder pressure contributed to the compression of the defects, and the defects were eliminated by increasing the pressure at the phase transition position. A significantly refined equiaxed microstructure with an average grain size of ∼0.9 μm was achieved below the β-phase transition temperature in the stir zone via back heating assisted FSW, while a bimodal structure with an average grain size of 3.5 μm was formed near the β-phase transition temperature. Inconspicuous reduction of the strength was detected for the joints (98 % of the BM) which possess equiaxed microstructures, and the corrosion resistance of the joints was enhanced compared to the BM. This superior synergy of mechanical and corrosion properties exceeded the majority of Ti alloy joints previously reported. This study provided an effective method for obtaining medium-thickness Ti alloy joints with ultrafine equiaxial structures with superior mechanical properties and corrosion resistance.
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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