SEM-DIC 表征 AlSi10Fe0.7 铸造合金在微结构尺度上的损伤机制

IF 4.8 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2024-10-20 DOI:10.1016/j.matchar.2024.114478
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引用次数: 0

摘要

商用铸造铝合金中存在各种脆性相,对其机械性能有很大影响。其中,硅析出物几乎无处不在,因为硅是一种常见的合金元素。在二次合金中,通常无法避免含铁相,它们往往会降低机械性能。本文对 Al-Si-Fe相体系(β-Al5FeSi)中硅相和失效临界金属间相之间的相互作用进行了高分辨率研究。该合金由大晶粒铝基体、硅沉淀物和板状 β-Al5FeSi 相组成。研究的目的是确定微观结构中的 "热点",在机械加载条件下,裂纹可能从这些 "热点 "中产生。主要工具是通过扫描电子显微镜(SEM-DIC)中的数字图像相关性进行变形分析。这样就能以高分辨率识别和跟踪不同潜在裂纹起始点的应变定位,并捕捉整个试样的全貌。经过调整的帧平均脚本将漂移引起的测量误差降至最低。SEM-DIC 的结果表明,变形场是由微结构成分的弹性不相容性决定的。裂纹的产生是由于 Si + β-Al5FeSi 相界的脱离。裂纹随后穿过相界,并沿着 β-Al5FeSi 相中的孪生边界扩展。最终的破坏是由断裂的脆性板状颗粒连接造成的。
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SEM-DIC characterization of the damage mechanism of an AlSi10Fe0.7 casting alloy on the microstructure scale
Various brittle phases are present in commercial cast aluminum alloys, which strongly influence their mechanical behavior. Among these, silicon precipitates are nearly omnipresent, as Si is a common alloying element. In secondary alloys, usually Fe-containing phases cannot be avoided, and they tend to degrade the mechanical properties. The interaction between the silicon phase and the failure-critical intermetallic phase in the Al-Si-Fe phase system (β-Al5FeSi) is studied in this paper in high resolution. A model alloy AlSi10Fe0.7 was defined, which is composed of a large grain Al-matrix, Si-precipitates and the plate-like β-Al5FeSi phase. The goal of the study was to identify “hot spots” in the microstructure from which cracks may initiate under mechanical loading. The main tool was a deformation analysis via digital image correlation in the SEM (SEM-DIC). This allows the identification and tracking of developing strain localizations at different potential crack initiation sites with a high resolution as well as capturing an overview over the whole specimen. An adapted frame averaging script minimized measurement errors induced by drift. The SEM-DIC results show that the deformation field is governed by the elastic incompatibility of the microstructural constituents. Crack initiation occurs because of the detachment of the Si + β-Al5FeSi phase boundary. Cracks then cross the phase boundary and propagate along twin boundaries in the β-Al5FeSi phase. Final failure is caused by linking fractured brittle plate-like particles.
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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