利用中等能量离子进行样品合成、制备和改性以及原位深度剖析的新系统

IF 3.8 2区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Vacuum Pub Date : 2024-11-09 DOI:10.1016/j.vacuum.2024.113824
Radek Holeňák , Dmitrii Moldarev , Eleni Ntemou , Theofanis Tsakiris , Carolin Frank , Kevin Vomschee , Svenja Lohmann , Daniel Primetzhofer
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引用次数: 0

摘要

我们在乌普萨拉大学 Tandem 实验室国家研究基础设施的离子注入器设备上展示了用于样品合成、制备和改性的设备,这些设备能够利用中等能量离子束进行原位研究。这些完整的仪器可实现可控薄膜合成、改性和表征,适用于研究薄膜生长、相变、氧化、退火、催化或离子注入等近表面过程。我们介绍了现有的仪器及其规格,并展示了四项演示实验,重点是已获得的原位能力,包括 1) 薄膜的蒸发和热合金化--硅化镍 2) 反应磁控溅射和离子注入。2) 反应磁控溅射和受控氧化--光致变色 YHO 3) 溅射和低能植入--钨中的氢和 4) 敏感系统的表面清洁--自支撑硅膜。
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A new system for sample synthesis, preparation and modification combined with in-situ depth profiling using medium energy ions
We present equipment for sample synthesis, preparation and modification enabling in-situ studies employing medium energy ion beams at the ion implanter facility of the Tandem Laboratory national research infrastructure at Uppsala University. The integral instrumentation enables controlled thin-film synthesis, modification and characterization applicable to study near-surface processes such as thin-film growth, phase transformation, oxidation, annealing, catalysis or ion implantation. We describe the available instrumentation with its specifications and present four demonstrative experiments with a particular focus on the acquired in-situ capabilities addressing 1) Evaporation and thermal alloying of thin films – nickel silicides 2) Reactive magnetron sputtering and controlled oxidization – photochromic YHO 3) Sputtering and low-energy implantation – hydrogen in tungsten and 4) Surface cleaning of sensitive systems – self-supporting silicon membranes.
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来源期刊
Vacuum
Vacuum 工程技术-材料科学:综合
CiteScore
6.80
自引率
17.50%
发文量
0
审稿时长
34 days
期刊介绍: Vacuum is an international rapid publications journal with a focus on short communication. All papers are peer-reviewed, with the review process for short communication geared towards very fast turnaround times. The journal also published full research papers, thematic issues and selected papers from leading conferences. A report in Vacuum should represent a major advance in an area that involves a controlled environment at pressures of one atmosphere or below. The scope of the journal includes: 1. Vacuum; original developments in vacuum pumping and instrumentation, vacuum measurement, vacuum gas dynamics, gas-surface interactions, surface treatment for UHV applications and low outgassing, vacuum melting, sintering, and vacuum metrology. Technology and solutions for large-scale facilities (e.g., particle accelerators and fusion devices). New instrumentation ( e.g., detectors and electron microscopes). 2. Plasma science; advances in PVD, CVD, plasma-assisted CVD, ion sources, deposition processes and analysis. 3. Surface science; surface engineering, surface chemistry, surface analysis, crystal growth, ion-surface interactions and etching, nanometer-scale processing, surface modification. 4. Materials science; novel functional or structural materials. Metals, ceramics, and polymers. Experiments, simulations, and modelling for understanding structure-property relationships. Thin films and coatings. Nanostructures and ion implantation.
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