Seong-Ho Lee , Chitturi Veerendra , Hyo-Sun Jang , Geon Young Lee , Ji Hoon Kim , Jae-Hyung Cho
{"title":"基于错向测量和晶界信息的冷轧 A1050 薄板再结晶行为研究","authors":"Seong-Ho Lee , Chitturi Veerendra , Hyo-Sun Jang , Geon Young Lee , Ji Hoon Kim , Jae-Hyung Cho","doi":"10.1016/j.msea.2024.147467","DOIUrl":null,"url":null,"abstract":"<div><div>The recrystallization behaviors of severely cold-rolled A1050 thin sheets (<span><math><mrow><mn>100</mn><mspace></mspace><mi>μ</mi><mi>m</mi></mrow></math></span> thick) with a reduction area of 98.3% were examined in detail. The thin sheets consisted of elongated and banded grain structures with typical <span><math><mi>β</mi></math></span>-fiber (Brass-S-Copper) texture components. Based on electron backscatter diffraction (EBSD), microstructural features such as misorientation measures of the kernel average misorientation (KAM) and grain boundary information of the lattice misorientation angle and axis were characterized. The elongated grains with representative orientations near Copper and S components possessed slightly greater KAM values than those near Brass. During annealing, newly recrystallized grains mainly contained the representative orientations near Copper and S, as opposed to Brass. Low angle grain boundaries (LAGB) observed between the recrystallized and deformed <span><math><mi>β</mi></math></span>-fiber grains revealed the occurrence of subgrain growth. The typical recrystallization Cube and Goss textures were also found during annealing. An equi-axed Cube grain growing inside deformed grains with the representative orientation near Copper reveals widespread grain boundary misorientation. An ellipsoidal Goss texture grows up along the two deformed bands with equivalent near-S orientations. One band is mainly consumed by Goss, and the other band prevents it from growing inward by means of grain boundaries with 60<span><math><msup><mrow></mrow><mrow><mo>∘</mo></mrow></msup></math></span> <span><math><mrow><mo>〈</mo><mn>111</mn><mo>〉</mo></mrow></math></span>. Various grain boundary misorientations reveal the dynamic evolution of the newly recrystallized grains.</div></div>","PeriodicalId":385,"journal":{"name":"Materials Science and Engineering: A","volume":"920 ","pages":"Article 147467"},"PeriodicalIF":6.1000,"publicationDate":"2024-11-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Investigation of the recrystallization behavior of cold-rolled A1050 thin sheets based on misorientation measurements and grain boundary information\",\"authors\":\"Seong-Ho Lee , Chitturi Veerendra , Hyo-Sun Jang , Geon Young Lee , Ji Hoon Kim , Jae-Hyung Cho\",\"doi\":\"10.1016/j.msea.2024.147467\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>The recrystallization behaviors of severely cold-rolled A1050 thin sheets (<span><math><mrow><mn>100</mn><mspace></mspace><mi>μ</mi><mi>m</mi></mrow></math></span> thick) with a reduction area of 98.3% were examined in detail. The thin sheets consisted of elongated and banded grain structures with typical <span><math><mi>β</mi></math></span>-fiber (Brass-S-Copper) texture components. Based on electron backscatter diffraction (EBSD), microstructural features such as misorientation measures of the kernel average misorientation (KAM) and grain boundary information of the lattice misorientation angle and axis were characterized. The elongated grains with representative orientations near Copper and S components possessed slightly greater KAM values than those near Brass. During annealing, newly recrystallized grains mainly contained the representative orientations near Copper and S, as opposed to Brass. Low angle grain boundaries (LAGB) observed between the recrystallized and deformed <span><math><mi>β</mi></math></span>-fiber grains revealed the occurrence of subgrain growth. The typical recrystallization Cube and Goss textures were also found during annealing. An equi-axed Cube grain growing inside deformed grains with the representative orientation near Copper reveals widespread grain boundary misorientation. An ellipsoidal Goss texture grows up along the two deformed bands with equivalent near-S orientations. One band is mainly consumed by Goss, and the other band prevents it from growing inward by means of grain boundaries with 60<span><math><msup><mrow></mrow><mrow><mo>∘</mo></mrow></msup></math></span> <span><math><mrow><mo>〈</mo><mn>111</mn><mo>〉</mo></mrow></math></span>. Various grain boundary misorientations reveal the dynamic evolution of the newly recrystallized grains.</div></div>\",\"PeriodicalId\":385,\"journal\":{\"name\":\"Materials Science and Engineering: A\",\"volume\":\"920 \",\"pages\":\"Article 147467\"},\"PeriodicalIF\":6.1000,\"publicationDate\":\"2024-11-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Science and Engineering: A\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0921509324013984\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Science and Engineering: A","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0921509324013984","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
摘要
详细研究了减薄面积为 98.3% 的严重冷轧 A1050 薄板(100μm 厚)的再结晶行为。这些薄板由细长的带状晶粒结构组成,具有典型的β-纤维(黄铜-S-铜)纹理成分。基于电子反向散射衍射 (EBSD),对微观结构特征进行了表征,如核平均失向度 (KAM) 的失向测量以及晶格失向角和轴的晶界信息。铜和 S 成分附近具有代表性取向的细长晶粒的 KAM 值略大于黄铜附近的晶粒。在退火过程中,新再结晶的晶粒主要包含铜和 S 附近的代表性取向,而不是黄铜附近的代表性取向。在再结晶和变形 β 纤维晶粒之间观察到的低角度晶界 (LAGB) 显示了亚晶粒生长的发生。退火过程中还发现了典型的再结晶立方体和戈斯纹理。等轴立方体晶粒生长在变形晶粒内部,其代表取向接近铜,显示出广泛的晶界错向。一个椭圆形的 Goss 纹理沿着两个具有等效近 S 取向的变形带生长。一条变形带主要被戈斯纹理吞噬,另一条变形带则通过 60∘ 〈111〉的晶界阻止戈斯纹理向内生长。各种晶界错向揭示了新再结晶晶粒的动态演变。
Investigation of the recrystallization behavior of cold-rolled A1050 thin sheets based on misorientation measurements and grain boundary information
The recrystallization behaviors of severely cold-rolled A1050 thin sheets ( thick) with a reduction area of 98.3% were examined in detail. The thin sheets consisted of elongated and banded grain structures with typical -fiber (Brass-S-Copper) texture components. Based on electron backscatter diffraction (EBSD), microstructural features such as misorientation measures of the kernel average misorientation (KAM) and grain boundary information of the lattice misorientation angle and axis were characterized. The elongated grains with representative orientations near Copper and S components possessed slightly greater KAM values than those near Brass. During annealing, newly recrystallized grains mainly contained the representative orientations near Copper and S, as opposed to Brass. Low angle grain boundaries (LAGB) observed between the recrystallized and deformed -fiber grains revealed the occurrence of subgrain growth. The typical recrystallization Cube and Goss textures were also found during annealing. An equi-axed Cube grain growing inside deformed grains with the representative orientation near Copper reveals widespread grain boundary misorientation. An ellipsoidal Goss texture grows up along the two deformed bands with equivalent near-S orientations. One band is mainly consumed by Goss, and the other band prevents it from growing inward by means of grain boundaries with 60 . Various grain boundary misorientations reveal the dynamic evolution of the newly recrystallized grains.
期刊介绍:
Materials Science and Engineering A provides an international medium for the publication of theoretical and experimental studies related to the load-bearing capacity of materials as influenced by their basic properties, processing history, microstructure and operating environment. Appropriate submissions to Materials Science and Engineering A should include scientific and/or engineering factors which affect the microstructure - strength relationships of materials and report the changes to mechanical behavior.