Stefano Felicioni , Elisa Padovano , Federica Bondioli , Paolo Fino
{"title":"通过电子束粉末床熔化获得的 CuCrZr 合金:微观结构见解和沉淀行为","authors":"Stefano Felicioni , Elisa Padovano , Federica Bondioli , Paolo Fino","doi":"10.1016/j.matchar.2024.114559","DOIUrl":null,"url":null,"abstract":"<div><div>An in-depth characterization of microstructure and mechanical properties of CuCrZr alloy processed by electron beam powder bed fusion (EB-PBF) additive manufacturing technology was performed with the aim to investigate the effect the thermal history of the material during the building process has on the properties of printed parts. Fully dense samples with a relative density up to 99.77 ± 0.04 % were successfully obtained in optimized conditions. The samples in the as-built condition exhibit an anisotropic microstructure dependent on the energetic input. An extensive microstructural transformation occurs alongside the precipitation and segregation of chromium-rich species, driven by the elevated thermal conditions during the deposition process. This unique thermal evolution can be properly investigated and exploited to eliminate the need for further post-processing heat treatments. To identify and quantify the precipitations within the microstructure, scanning and transmission electron microscopy together with electron backscattered diffraction were used.</div></div>","PeriodicalId":18727,"journal":{"name":"Materials Characterization","volume":"218 ","pages":"Article 114559"},"PeriodicalIF":4.8000,"publicationDate":"2024-11-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"CuCrZr alloy obtained via electron-beam powder bed fusion: Microstructural insights and precipitation behaviour\",\"authors\":\"Stefano Felicioni , Elisa Padovano , Federica Bondioli , Paolo Fino\",\"doi\":\"10.1016/j.matchar.2024.114559\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><div>An in-depth characterization of microstructure and mechanical properties of CuCrZr alloy processed by electron beam powder bed fusion (EB-PBF) additive manufacturing technology was performed with the aim to investigate the effect the thermal history of the material during the building process has on the properties of printed parts. Fully dense samples with a relative density up to 99.77 ± 0.04 % were successfully obtained in optimized conditions. The samples in the as-built condition exhibit an anisotropic microstructure dependent on the energetic input. An extensive microstructural transformation occurs alongside the precipitation and segregation of chromium-rich species, driven by the elevated thermal conditions during the deposition process. This unique thermal evolution can be properly investigated and exploited to eliminate the need for further post-processing heat treatments. To identify and quantify the precipitations within the microstructure, scanning and transmission electron microscopy together with electron backscattered diffraction were used.</div></div>\",\"PeriodicalId\":18727,\"journal\":{\"name\":\"Materials Characterization\",\"volume\":\"218 \",\"pages\":\"Article 114559\"},\"PeriodicalIF\":4.8000,\"publicationDate\":\"2024-11-19\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Characterization\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1044580324009409\",\"RegionNum\":2,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"MATERIALS SCIENCE, CHARACTERIZATION & TESTING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Characterization","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1044580324009409","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, CHARACTERIZATION & TESTING","Score":null,"Total":0}
CuCrZr alloy obtained via electron-beam powder bed fusion: Microstructural insights and precipitation behaviour
An in-depth characterization of microstructure and mechanical properties of CuCrZr alloy processed by electron beam powder bed fusion (EB-PBF) additive manufacturing technology was performed with the aim to investigate the effect the thermal history of the material during the building process has on the properties of printed parts. Fully dense samples with a relative density up to 99.77 ± 0.04 % were successfully obtained in optimized conditions. The samples in the as-built condition exhibit an anisotropic microstructure dependent on the energetic input. An extensive microstructural transformation occurs alongside the precipitation and segregation of chromium-rich species, driven by the elevated thermal conditions during the deposition process. This unique thermal evolution can be properly investigated and exploited to eliminate the need for further post-processing heat treatments. To identify and quantify the precipitations within the microstructure, scanning and transmission electron microscopy together with electron backscattered diffraction were used.
期刊介绍:
Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials.
The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal.
The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include:
Metals & Alloys
Ceramics
Nanomaterials
Biomedical materials
Optical materials
Composites
Natural Materials.