Ti-47.5Al-2.5 V-1.0Cr-0.2Zr合金高温拉伸本构行为及变形机理研究

IF 4.8 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2024-12-01 DOI:10.1016/j.matchar.2024.114594
Xuejian Lin , Xin Liu , Hongjun Huang , Bowen Zheng , Kai Du , Xiaojiao Zuo , Xiaoguang Yuan
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引用次数: 0

摘要

采用电子万能试验机对Ti-47.5Al-2.5 V-1.0Cr-0.2Zr合金在750 ~ 900℃/10−5 ~ 3 s−1条件下进行了高温拉伸试验。分析了热拉应力-应变曲线,建立了热拉条件下的本构模型。确定了拉伸过程中的组织转变规律和变形机理。结果表明:较低的应变速率和较高的拉伸温度使稳态流动阶段的热拉伸曲线变长,真实应力减小,断裂伸长率增大;根据拉伸曲线数据建立本构方程,得到相应的热活化能为310.3 kJ/mol。随着拉伸温度的升高和应变速率的降低,跨层断口在拉伸断口形貌中所占的比例降低,韧窝数量增加,更多的片层组织转变为再结晶组织,合金的软化效果更加明显。位错变形机制主要包括位错滑移和攀升的存在、位错相交和位错环或位错网络的形成。孪晶变形也是TiAl合金高温拉伸变形的另一重要机理。孪晶相互平行形成,使变形进一步进行。变形组织中的位错和孪晶为晶粒的再结晶提供了形核条件。动态再结晶(DRX)晶粒优先在晶界附近形成,位错和孪晶附近也是DRX的优先成核部位。DRX行为是主要的软化机制,低拉伸速率和高拉伸温度对应的DRX尺寸和体积分数较大。
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Study on high temperature tensile constitutive behavior and deformation mechanism of Ti-47.5Al-2.5 V-1.0Cr-0.2Zr alloy
The high temperature tensile test of Ti-47.5Al-2.5 V-1.0Cr-0.2Zr alloy was carried out by electronic universal testing machine under the condition of 750–900 °C/10−5–10−3 s−1. The hot tensile stress-strain curves were analyzed, and the constitutive model under hot tensile conditions was established. The microstructure transformation rule and deformation mechanism during tensile process were determined. The results show that the hot tensile curve is longer in the steady-state flow stage corresponding to lower strain rate and higher tensile temperature, the true stress declines and the elongation at break increases. The constitutive equation was established based on the tensile curve data, and the corresponding thermal activation energy was 310.3 kJ/mol. As the rise of tensile temperature and the decline of strain rate, the proportion about cross-layer fracture in the tensile fracture morphology decreases, the number of dimples increases, more lamellar structures change into recrystallized structures, and the softening effect of the alloy is more obvious. The dislocation deformation mechanism mainly includes the existence of dislocation slip and climb, dislocation intersection and dislocation ring or dislocation network formation. Twinning deformation is also another important mechanism of high temperature tensile deformation of TiAl alloy. Twins are formed in parallel with each other, so that the deformation can be further carried out. The dislocations and twins in the deformed microstructure will provide nucleation conditions for recrystallized grains. The dynamic recrystallization(DRX) grains are preferentially formed around the grain boundary and the vicinity of dislocation and twin is also preferred nucleation site for DRX. The DRX behavior is the main softening mechanism, and DRX size and volume fraction corresponding to lower tensile rate and higher tensile temperature are larger.
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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