{"title":"MIL-91(Al)晶体结构的再测定。","authors":"Nele Hermer, Michael T Wharmby, Norbert Stock","doi":"10.1002/zaac.201600358","DOIUrl":null,"url":null,"abstract":"<p><p>The structure of one of the first permanently porous metal phosphonates, MIL-91(Al) was re-determined using high resolution synchrotron powder X-ray diffraction data. The new model is in a lower symmetry space group, with no disordered ligands in the structure, whilst remaining otherwise consistent with the reported compound. New milder synthetic conditions were also developed.</p>","PeriodicalId":54398,"journal":{"name":"Zeitschrift fur Anorganische und Allgemeine Chemie","volume":"643 2","pages":"137-140"},"PeriodicalIF":1.1000,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/zaac.201600358","citationCount":"8","resultStr":"{\"title\":\"Re-Determination of the Crystal Structure of MIL-91(Al).\",\"authors\":\"Nele Hermer, Michael T Wharmby, Norbert Stock\",\"doi\":\"10.1002/zaac.201600358\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>The structure of one of the first permanently porous metal phosphonates, MIL-91(Al) was re-determined using high resolution synchrotron powder X-ray diffraction data. The new model is in a lower symmetry space group, with no disordered ligands in the structure, whilst remaining otherwise consistent with the reported compound. New milder synthetic conditions were also developed.</p>\",\"PeriodicalId\":54398,\"journal\":{\"name\":\"Zeitschrift fur Anorganische und Allgemeine Chemie\",\"volume\":\"643 2\",\"pages\":\"137-140\"},\"PeriodicalIF\":1.1000,\"publicationDate\":\"2017-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1002/zaac.201600358\",\"citationCount\":\"8\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Zeitschrift fur Anorganische und Allgemeine Chemie\",\"FirstCategoryId\":\"92\",\"ListUrlMain\":\"https://doi.org/10.1002/zaac.201600358\",\"RegionNum\":4,\"RegionCategory\":\"化学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"2016/12/16 0:00:00\",\"PubModel\":\"Epub\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, INORGANIC & NUCLEAR\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Zeitschrift fur Anorganische und Allgemeine Chemie","FirstCategoryId":"92","ListUrlMain":"https://doi.org/10.1002/zaac.201600358","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2016/12/16 0:00:00","PubModel":"Epub","JCR":"Q4","JCRName":"CHEMISTRY, INORGANIC & NUCLEAR","Score":null,"Total":0}
Re-Determination of the Crystal Structure of MIL-91(Al).
The structure of one of the first permanently porous metal phosphonates, MIL-91(Al) was re-determined using high resolution synchrotron powder X-ray diffraction data. The new model is in a lower symmetry space group, with no disordered ligands in the structure, whilst remaining otherwise consistent with the reported compound. New milder synthetic conditions were also developed.
期刊介绍：
ZAAC is an international scientific journal which publishes original papers on new relevant research results from all areas of inorganic chemistry, solid state chemistry, and co-ordination chemistry.
The contributions reflect the latest findings in these research areas and serve the development of new materials, such as super-hard materials, electrical superconductors, or intermetallic compounds. Up-to-date physical methods for the characterization of new chemical compounds and materials are also described.
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