医用AlTiN涂层摩擦学和电化学性能的影响

IF 0.1 Q4 ENGINEERING, CHEMICAL Journal of the Pakistan Institute of Chemical Engineers Pub Date : 2021-03-26 DOI:10.54693/piche.04911
H. Sajjad, M. U. Manzoor, H. Zafar, Khurram Shahzad, Faraz Hussain
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引用次数: 0

摘要

物理气相沉积技术一直是在不同金属基底上沉积金属和陶瓷涂层的重要技术。通过使用至少2个带靶的横向旋转阴极,可以改善物理气相沉积镀膜工艺中的辉光放电过程。采用横向电弧旋转阴极(LARC)技术在生物医学植入体不锈钢样品上沉积AlTiN涂层。阴极的横向旋转使阴极在镀膜腔内均匀消耗,从而获得最大的成品率。采用扫描电镜(SEM)和能量色散x射线能谱(EDX)对涂层的均匀性和厚度进行了表征。采用开路电位(OCP)、电化学阻抗谱(EIS)和循环极化测试对其在乳酸林格溶液中的腐蚀行为进行了表征。在三种不同载荷下进行了摩擦学测试,以评估涂层的摩擦系数。电化学测试表明,涂层样品的耐蚀性优于未涂层的基底,表现出阴极保护涂层的特性,并具有更高的电阻率。摩擦学试验也表明,相对于施加的载荷,涂层质量得到了改善。
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Effect of Tribological and Electrochemical properties of AlTiN Coating for Medical Application
Physical Vapor Deposition technique is always an important technique to deposit metallic and ceramic coatings on different metallic substrates. The glow discharge process can be improved in a physical vapor deposition coating process by using least 2 lateral rotating cathodes with targets. Lateral Arc Rotating Cathode (LARC) technology was used to deposit AlTiN coating on stainless steel samples for biomedical implant application. The lateral rotation of cathode makes the uniform consumption of the cathodes in the coating chamber to get the maximum yield. The coating was characterized by Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDX) for their uniformity and thickness. Open circuit potential (OCP), Electrochemical Impedance Spectroscopy (EIS) and Cyclic polarization test were performed for their corrosion behavior in ringer lactate solution. Tribological testing was also performed at three different load to evaluate the coefficient of friction of the coating. The Electrochemical tests indicated that corrosion resistance of the coated sample was better, than the uncoated substrate and it behaved like cathodically protected coating and showed more resistivity. The tribological test also showed improved coating quality with respect to the applied load.
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